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I <br /> 1. <br /> L <br /> L05/10/07 10:16 <br /> Kleinfelder(Stockton) Project: Kenworth T-22 <br /> 2825 East Myrtle St, Project Number: 82946.H01 CLS Work Order#:CQE0105 <br /> L Stockton,CA 95205 Project Manager: Joseph D.Zilles COC#:3997,3998,3999 <br /> DRAFT: Metals (Dissolved) by EPA 200 Series Methods- Quality Control <br /> V Reporting Spike Source %REC RPD <br /> Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes <br /> Batch CQ03782-EPA 3010A <br /> L <br /> LES Dup(CQ03782-BSDl) Prepared&Analyzed:05/03/07 <br /> Aluminum 1820 50 pg/L 2000 91.0 80-120 0.772 20 <br /> Barium 2000 100 2000 99.8 80-120 0.402 20 <br /> Boron 2480 100 " 2500 99.1 80-120 0.526 20 <br /> Beryllium 50.2 1.0 " 50.0 100 80-120 0.981 20 <br /> Chromium 205 10 200 102 80-120 4.09 20 <br /> ` Copper 247 50 250 98.6 80-120 0.896 20 <br /> Iron 1020 100 1000 102 80-120 1.39 20 <br /> Manganese 501 10 " 500 100 80-120 0.520 20 <br /> Nickel 502 10 500 100 80-120 0.00 20 <br /> to Silver 48.1 10 50.0 96.2 80-120 2.74 20 <br /> Zinc 502 50 500 100 80-120 1.24 20 <br /> Matrix Spike(CQ03782-MS1) Source:CQE0105-02 Prepared&Analyzed:05/03/07 <br /> Aluminum 1840 50 pg/L 2000 ND 92.2 75-125 <br /> Barium 2170 100 2000 176 99.5 75-125 <br /> Boron 2700 l00 2500 249 98.1 75-125 <br /> Beryllium 50.3 1.0 50.0 ND 101 75-125 <br /> Chromium 207 10 200 ND 104 75-125 <br /> Copper 253 50 250 11.4 96.8 75-125 <br /> Iron 1290 100 " 1000 298 99.4 75-125 <br /> Manganese 497 10 500 2.90 98.7 75-125 <br /> Nickel 493 10 500 ND 98.5 75-125 <br /> } Silver 47.0 10 50.0 ND 94.0 75-125 <br /> Zinc 544 50 500 50.7 98.7 75-125 <br /> Matrix Spike Dup(CQ03782-MSD1) Source:CQE0105-02 Prepared&Analyzed:05/03/07 <br /> ` Aluminum 1850 50 pg/L 2000 ND 92.7 75-125 0.595 25 <br /> 6. Barium 2200 100 2000 176 101 75-125 1.33 25 <br /> Boron 2730 100 2500 249 99.2 75-125 0.994 25 <br /> L Beryllium 50.8 1.0 11 50.0 ND 102 75-125 0.811 25 <br /> Chromium 207 10 200 ND 104 75-125 0.00 25 <br /> Copper 253 50 250 11.4 96.8 75-125 0.00 25 <br /> Iron 1300 100 1000 298 100 75-125 0.386 25 <br /> L Manganese 500 t0 ii 500 2.90 99.5 75-125 0.722 25 <br /> Nickel 496 10 500 ND 99.3 75-125 0.748 25 <br /> Silver 46.0 10 50.0 ND 92.0 75-125 2.15 25 <br /> LZinc 546 50 500 50.7 99.0 75-125 0.275 25 <br /> L <br /> LCA DOHS FLAP Accreditation/Registration Number 1233 PLATE <br /> 37 <br />