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r <br /> I 10 Second Avenue South,#D7,Pacheco,CA 94553 <br /> McCAMPBELL ANALYTICAL INC Telephone 510-798-1620 Fax 510-798-1622 <br /> httii//www mccampbell com E-mail main@mccampbell corn <br /> GEOSOLV,Inc Client Project ID Nunan, Highway 88, Date Sampled 08/12/97 <br /> Lockeford Date Received 08/13/97 <br /> 643 Oregon Street <br /> Sonoma,CA 95476 Client Contact Frank Goldman Date Extracted 08/13/97 <br /> Client P O Date Analyzed 08113-08/15/97 <br /> Volatile Organics By GUMS <br /> EPA method 8260 <br /> Lab ID 79742 <br /> Client ID 135-2 <br /> Matrix S <br /> Compound Concentration* Compound Concentration* <br /> Acetone ND<20 trans-i,3-Dtchloropropene ND<20 <br /> Benzene ND<20 Ethylene dibromide ND<20 <br /> Bromobenzene ND<20 Ethylbenzene 58 <br /> Bromochloromethane ND<20 Hexachlorobutadiene ND<20 <br /> Bromodichloromethane ND<20 lodomethane ND<20 <br /> Bromofoim ND<20 lsopropylbenzene ND<20 <br /> Bromomethane ND<20 p4sopropyl toluene 58 <br /> n-Butyl benzene ND<20 Methyl butyl ketone ND<20 <br /> sec-Butyl benzene ND<20 Methyiene Chloride ND<20 <br /> tert-Butyl benzene ND<20 Methyl ethyl ketones ND<20 <br /> Carbon Disulfide ND<20 Methyl isoburyl ketone ND<20 <br /> Carbon Tetrachloride ND<20 Methyl tert-Butyl Ether(MTBE) NI3<20 <br /> Chiorobenzene ND<20 Napthalene ND<25 <br /> Chloroethane ND<20 n-Propyl benzene 41 <br /> 2-Chloroethyl Vinyl Ether"' N0<20 Styrene ND<20 <br /> Chloroform ND<20 1,1 1 2-Tetrachloroethane ND<20 <br />' Chloromethane ND<20 1,1 2 2-Tetrachloroethane ND<20 <br /> 2-Chlorotoluene ND<20 Tetrachioroethene ND<20 <br /> 4-Chlorotoluene ND<20 Toluene"" ND<20 <br /> Dibromochloromethane ND<20 1,2 3-Trichlorobenzene ND<20 <br /> 1,2-Dibromo-3-chloropropane ND<20 12,4-Trichlorobenzene ND<20 <br /> Dibromomethane ND<20 1,1,1-Trichloroethane NLK20 <br /> 1,2-Dichlorobenzene ND<20 1 1 2-Trichloroethane ND<20 <br /> 1,3-Dichiorobenzene ND<20 Trichloroethene ND<20 <br /> 1,4-Dichlorobenzene ND<20 Trichlorofluoromethane ND<20 <br /> Dieblorodifluoromcthane ND<20 1,2,3-Trichloropropane ND<20 <br /> 1,I-Dichloroethane ND<20 1,2 4-Trimethyibenzene 420 <br /> 1,2-Dichloroethane ND<20 1,3,5-Trimethylbenzene 110 <br /> LI-Dichlormthene ND<20 Vinyl Acetate "' ND<20 <br /> cis-1,2-Dichloroethene ND<20 Vinyl Chloride ° ND<20 <br /> trans-1,2-Dichloroethene ND<20 Xylenes total r 230 <br /> 1,2-Dichloropropane ND<20 Comments <br /> 1,3-Dichloropropane ND<20 Surrogate Recoveries(%) <br /> 2,2-Dichloropropane ND<20 Dibromofluoromethane 84 <br /> 1,1-Dtchloropropene ND<20 Toluene-d8 102 <br /> cis-1,3-Dtchloropropene ND<20 4-Bromofluorobenzene 118 <br /> 'water and vapor samples are reported in ug/L,soil and sludge samples in ug/kg wipes in ug/wipe and all TCLP I SDLP extracts in ug/L <br /> Reporting limits unless otherwise stated water samples 1 ug/L vapor samples 0 5 ug/L,solid and sludge samples 5 ug/kg,wipes 0 2ug/wipe <br /> ND means not detected above the reporting limit,NIA means analyte not applicable to this analysis <br /> (b) 2-propanone or dimethyl ketone, (c) (2-chloroethoxy) ethene (d) 2-hexanone (c) dtchloromethane, (f) 2-butanone, (g) 4-methyl-2- <br /> pentanone or isopropylacetone,(h)lighter than water immiscibie sheen is present (i) liquid sample that contains greater than---5 vol % <br /> sediment, 0) sample diluted due to high organic content, (k) ethenylbenzene (1) methylbenzene (m) acetic acid ethenyl ester, (n) <br /> chloroethene,(o)dimethylbenzenes <br /> DHS Certification No 1644 Edward Hamilton,Lab Director <br />