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110 Second Avenue South,#D7,Pacheco,CA 94553 <br /> McCAMPBELL ANALYTICAL INC Telephone 510-798-1620 Fax 510-798-1622 <br /> http//www mccampbell_corn E-mail main@mccampbell corn <br />' GEOSOLV, Inc Client Project ID Nunan,Highway 88, Date Sampled 08/12/97 <br /> Lockeford Date Received 08/13/97 <br />' 643 Oregon Street <br /> Sonoma,CA 95476 Client Contact Frank Goldman Date Extracted 08/13/97 <br /> Client P O Date Analyzed 08/13-08/15/97 <br /> Volatile Organics By GCIMS <br /> EPA method 8260 <br /> Lab ID 79753 <br /> Client ID 134-2 <br /> Matrix S <br /> Compound Concentration* Compound Concentration* <br /> Acetone ND<700 trans-l,3-Dichloropropene NIK700 <br /> Benzene ND<700 Ethylene dibromide ND<700 <br /> Bromobenzene ND<700 Ethylbenzene 6900 <br /> Bromochloromethane ND<700 Hexachlorobutadiene ND<700 <br /> Bromodichloromethanc NDK700 lodomethane ND<700 <br /> Bromoform ND<700 Isopropylbenzene 970 <br /> Bromomethane ND<700 p-Isopropyl toluene ND<700 <br /> n-Butyl benzene ND<700 Methyl butyl ketone" ND<700 <br /> sec-Butyl benzene ND<700 Methylene Chloride ND<700 <br /> tert-Butyl benzene ND<700 Methyl ethyl ketone'K' ND<700 <br /> Carbon Disulfide ND<700 Methyl isobutyl ketoneND<700 <br /> Carbon Tetrachloride ND<700 Methyl tert-Butyl Ether(MTBE) ND<700 <br /> Chlorobenzene ND<700 Napthaicnc ND<800 <br /> Chloroethane ND<700 n-Propyl benzene 3100 <br /> 2-Chloroethyl Vinyl Ethe ND<700 Styrene ND<700 <br /> Chloroform ND<700 1 1,1,2-Tetrachloroethane ND<700 <br />' Chloromethane ND<700 1,1 2 2-Tetrachloroethane ND<700 <br /> 2-Chlorotoiuene ND<700 Tetrachioroethene ND<700 <br /> 4-Chlorotoluene ND<700 Toluene 'W 4300 <br /> Dibromochloromethane ND<700 1,2 3-Tnchlorobenzene ND<700 <br /> 1,2-Dibromo-3-chloropropane ND<700 1,2 4-Tnchlorobenzene ND<700 <br /> Dibromomethane ND<700 1,1,1-Trichloroethane ND<700 <br /> 1,2-Dichlorobenzene ND<700 1,1,2-Trichi oroethane ND<700 <br /> 1,3-Dichlorobenzene ND<700 Trichloroethene ND<700 <br /> 1,4-Dichlorobenzene ND<700 Trichlorofluoromethane ND<700 <br /> Dichlorodifluoromethane ND<700 1 2 3-Tnchloropropane ND<700 <br /> 1,1-Dicbloroethane ND<700 1 2 4-rnmethylbenzen a 18,000 <br /> 1,2-Dichloroethane N13<700 1,3,5-Trimethylbenzene 5500 <br /> i,I-Dichloroethene ND<700 Vinyl Acetate "' ND<700 <br /> cis-1,2-Dichioroethene ND<700 Vinyl Chloride ND<700 <br /> trans-l,2-Dichloroethene ND<700 Xylenes,total " 40,000 <br /> 1,2-Dtchloropropane ND<700 Comments <br /> 1,3-Dichloropropane ND<700 Surrogate Recoveries(%) <br /> 2,2-Dtchloropropane NIK700 Dibromofluoromethane 94 <br /> 1,1-Dichlorepropene ND<700 Toluene-d8 94 <br /> cis-1,3-Dichloropropene ND<700 4-Bromolluorobenzene 120 <br /> 'water and vapor samples are reported in ug/L,soil and sludge samples in ug/kg wipes in ug/wipe and all TCLP/SPLP extracts in ug/L <br /> Reporting limits unless otherwise stated water samples I ug/L vapor samples 0 5 ug/L solid and sludge samples 5 ug/kg,wipes 0 2ug/wipe <br /> ND means not detected above the reporting limit,N/A means analyte not applicable,to this analysis <br /> (b) 2-propanone or dimethyl ketone, (c) (2-chloroethoxy) ethene (d) 2-hexanonc (e) dichloromethane, (n 2-butanone, (g) 4-methyl-2- <br /> pentanone or isopropylacetone, (h)lighter than water immiscible sheen is present (i) liquid sample that contains greater than —5 vol % <br /> sediment, 0) sample diluted due to high organic content (k) ethenylbenzene, (1) methylbenzene (m) acetic acid ethenyl ester, (n) <br /> chloroethene,(o)dimethylbenzenes p <br /> DHS Certification No 1644 #a✓ Edward Hamilton, Lab Director <br />