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CALIFORNIA LABORATORY SERVICES <br />'age 8 of 10 06/16/17 14:,3 <br />Precision Pnviro-Tcch Project: 7060818 <br />3935 N. Coronado Ave Project Number. 7060818 CLS Work Order#: 17FO416 <br />Stockton, CA 95204 Project Manager. Jonathan HV Lee COC k: <br />Acid and Base/Neutral EYtractables by EPA Method 625 - Quality Control <br />Reporting Spike Source %R CC RPD <br />lnalyte Result Limit Units Level Result %REC Limits RPD Limit Notes <br />Batch 1704375 - EPA 3510B GCMS <br />Source: 1700394-01 <br />Acenapluhene <br />715 <br />5000 µ81L <br />14.Dichlorobetuene <br />505 <br />5000 " <br />LCS Dup (1704375-BSDI) <br />265 <br />_ <br />Prepared: 06/14/17 Analyzed: 06/15/17 <br />--30- <br />5000 " <br />Acenaphthene <br />34.1 <br />10 pgIL <br />40.0 <br />85 <br />46.118 <br />10 <br />715 <br />1,4-Dichlorobenzene <br />24.1 <br />10 <br />40,0 <br />60 <br />36-117 <br />13 <br />30 <br />2,4Dinitrotoluette (2,4-DNT) <br />37.3 <br />10 <br />40.0 <br />93 <br />24-116 <br />8 <br />30 <br />N-Nitrosodi-n-propylamine <br />31.3 <br />10 <br />40.0 <br />78 <br />41.126 <br />11 <br />30 <br />Pyrene <br />39.4 <br />10 <br />40.0 <br />99 <br />26.127 <br />4 <br />30 <br />1,2,4-Trichlorobenzene <br />26.0 <br />10 <br />40.0 <br />65 <br />39-118 <br />12 <br />30 <br />4-Chloro-3-methylphenol <br />36.0 <br />20 <br />40.0 <br />90 <br />23-117 <br />6 <br />30 <br />2 -Chlorophenol <br />30.7 <br />10 <br />4o.0 <br />77 <br />23-134 <br />II <br />30 <br />4-Nittophenol <br />27.5 <br />25 <br />40.0 <br />69 <br />10.108 <br />5 <br />30 <br />Pentachlomphenol <br />40.8 <br />25 <br />40.0 <br />102 <br />9-113 <br />6 <br />30 <br />Phenol <br />21.1 <br />10 <br />40.0 <br />53 <br />5-112 <br />---21-110 <br />13 <br />30 <br />Surrogate; 2-lluarophenol <br />27.1 <br />40.0 - <br />68 <br />Surragate: Phenol -d6 <br />20.0 <br />40.0 <br />3t) <br />HI -1111 <br />Surrogate.- Nitrobewene-d5 <br />3113 <br />40.0 <br />81 <br />35-114 <br />Surrogate:2-17trorobtphcgI <br />30.7 <br />40.0 <br />77 <br />43-116 <br />Surmgare.- Z4,6-Trlbromophenol <br />39,1 <br />40.0 <br />98 <br />10.123 <br />Surrogate: TerphenyW14 <br />39.7 <br />40.0 <br />99 <br />33-141 <br />Matrix Spike. (1704375 -MSI) <br />- - <br />Source: 1700394-01 <br />Acenapluhene <br />715 <br />5000 µ81L <br />14.Dichlorobetuene <br />505 <br />5000 " <br />2,4.Dinitmtoluenc(2,4-DM) <br />265 <br />5000 " <br />N-Nitrosodi-n-propylamme <br />650 <br />5000 " <br />pyrone <br />615 <br />$000 <br />12,4-Trichlorobenzene <br />515 <br />5000 " <br />4-Chloro-3-methylphenol <br />715 <br />10000 " <br />2 -Chlorophenol <br />630 <br />5000 " <br />4-Nitrophenol <br />825 <br />13000 <br />Pentachlorophenol <br />1790 <br />13000 " <br />Phenol <br />470 <br />5000 " <br />Surrogate: 2-Fhroraphana4 <br />483 <br />" <br />Prepared: <br />06/14/17 Analyzed: <br />06//13/17 <br />800 <br />ND <br />89 <br />46.118 <br />800 <br />ND <br />63 <br />36-107 <br />Soo <br />ND <br />33 <br />24-106 <br />800 <br />ND <br />81 <br />41.116 <br />800 <br />ND <br />77 <br />26-127 <br />800 <br />ND <br />64 <br />39-98 <br />800 <br />ND <br />89 <br />23-107 <br />800 <br />ND <br />79 <br />27.123 <br />800 <br />ND <br />103 <br />10.100 <br />Soo <br />ND <br />224 <br />9-103 <br />800 <br />ND <br />59 <br />12-110 <br />- <br />San <br />-- <br />-6/ <br />21 -flu <br />QM -5 <br />QM -5 <br />CA DOHS ELAP Accreditation/Registmtion Number 1233 <br />3249 Fitzgerald Road Rancho Cordova, CA 95742 www.californialob.com 916-638-7301 Fax: 916-6384510 <br />