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Q UAL I T Y C O N T R O L R E S U L T S <br /> Job Number 992708 Report Date 01/06/2000 <br /> CUSTOMER IT Group PROJECT Southland - Martinez ATTN Rhonda Teicheira <br /> QC Type Description Reag Code Lab ID Dilution Factor Date Time <br /> MS Matrix Spike 09120705 992712-2 12/29/1999 0733 <br /> Parameter/Test Description QC Result QC Result True Value Orig Value Calc Result * Limits F <br /> Cert-But L Alcohol (TBA) - 698 69 1000 000000 0 69 9 34-182 <br /> i Isopropyl Ether 50 63 50 000000 0 101 3 60-131 <br /> Ethyl tert-Butyl Ether (ETRE) 45 11 50 000000 0 90 2 64-138 <br /> ert-AmY Y <br /> L Meth l Ether 43 53 50 000000 0 87 1 67-154 <br /> tl',2-DichLoroethane <br /> ethyL-t-Butyl Ether (MTBE) 88 92 100 000000 1 58 87 3 71-142 <br /> 9 08 10 000000 0 90 8 70-130 <br /> 1,2-Dtbromoethane (EDB) 8 94 10 000000 0 89 4 70-130 <br /> MSDMatrix Spike Duplicate 09120705 992712-2 12/29/1999 0805 <br /> Parameter/Test Description QC Result QC Result True Value Orig Value CaLc Result * Limits F <br /> tert-Butyl Alcohol (TBA) 848 55 698 69 1000 000000 0 84 9 34-182 <br /> 119 19 <br /> Di-IsopropyL Ether 54 80 50 63 50 000000 0 109 6 60'131 <br /> 8 24 <br /> tent-Butyl Ether (ETRE) 50 44 45 11 50 000000 0 100 9 64-138 <br /> 11 29 <br /> pt,rt-AnvyL Methyl Ether 49 43 43.53 50 000000 0 98 9 67-154 <br /> 13 27 <br /> Methyl-t-Butyl Ether (MTBE) 99 49 88 92 100.000000 1 58 97 9 71-142 <br /> 11 31 <br /> 11,2-DichLaroethane 9 96 9 08 10 000000 0 99 6 70-130 <br /> 9 30 <br /> 1,2-Dtbromoethane (EDB) 9 95 8 94 10 000000 0 99 5 70-130 <br /> 1 11 30 <br /> LCS Laboratory Control sample 09120705 12/29/19991139 <br /> Parameter/Test Description QC Result QC Result True Value Orig Value Calc Result * Limits F <br /> tert-Butyl Alcohol (TBA) 1049 09 1000 000000 104 9 37-175 <br /> Di-Isopropyl Ether 54 20 50 000000 108 4 60-138 <br /> Ethyl tert-Butyl Ether (ETBE) 50 80 50.000000 101 6 51-143 <br /> tert-Amyl Methyl Ether 51 52 50 000000 103 0 64-137 <br /> Methyt-t-Butyl Ether (MTBE) 105 27 100 000000 105 3 33-169 <br /> 1,2-Dichloroethane 10 04 10 000000 100 4 70-130 <br /> 1,2 Dtbromoethane (EDB) 10 16 10 000000 101 6 70-130 <br /> M8 Method Blank 12/29/1999 1213 <br /> Parameter/Test Description QC Result QC Result True Value Orig Value Calc Result limits F <br /> Itert-Butyl Alcohol (TBA) 14 64 <br /> Dt-isopropyl Ether 0 34 - <br /> ftert-AZrL <br /> thyl t-ButyL Ether (ETBE) 0 27 <br /> Methyl Ether 0 44 <br /> Wl-t-Butyl Ether (MTBE) 1 07 <br /> y�',chtoroethane 0 16 <br /> tbromoethane (EDB) 0 20 <br /> € I I Page 7 * %=% REC, R=RPD, A=ABS Diff D=% Diff., <br />