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COLUMBIA ANALYTICAL SERVICE. NC. <br /> Analytical Report <br /> Client: Equiva Services Service Request: K9904880 <br /> Project: Incident#88870583/SAP#121258 Date Collected: 6/29/99 <br /> Sample Matrix: Soil Date Received: 6/30/99 <br /> Date TCLP Performed: 7/27/99 <br /> Date Extracted: NA <br /> Date Analyzed: 7/29/99 <br /> Toxicity Characteristic Leaching Procedure(TCLP) <br /> EPA Method 1311 <br /> Volatile Organic Compounds <br /> Sample Name: SP-16AB COMP Units: mQiL,(ppm) <br /> Lab Code: K9904880-052 Basis: NA <br /> Test Notes: <br /> Prep Analysis Dilution Regulatory Result <br /> Analyte Method Method MRL Factor Limit* Result Notes <br /> Benzene EPA 1311 8260B 0.2 1 0.5 ND <br /> Carbon Tetrachloride EPA 1311 8260B 0.2 1 0.5 ND <br /> Chlorobenzene EPA 1311 8260B 0.2 1 100 ND <br /> Chloroform EPA 1311 8260B 0.2 1 6 ND <br /> 1,4-Dichlorobenzene EPA 1311 8260B 0.2 1 7.5 ND <br /> 1,2-Dichloroethane(EDC) EPA 1311 8260B 0.2 1 0.5 ND <br /> 1,1-Dichloroethene EPA 1311 8260B 0.2 1 0.7 ND <br /> 2-Butanone(MEK) EPA 1311 8260B 10 1 200 ND <br /> Tetrachloroethene(PCE) EPA 1311 8260B 0.2 1 0.7 ND <br /> Trichloroethene(TCE) EPA 1311 8260B 0.2 1 0.5 ND <br /> Vinyl Chloride EPA 1311 8260B 0.2 1 0.2 ND <br /> * From 40 CFR Part 261,et al.,and Federal Register,March 29,1990 and June 29, 1990. <br /> Approved By: Date: 0 - <br /> TCLP1S22/052595 <br /> Page 34 <br />