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885 Jarvis Drive <br /> Sequoia Morgan Hill CA 95037 <br /> (408)776-9" <br /> FAX(408)782-6308 <br /> Analytical www sequoialabs corn <br /> Blaine Tech Services(Shell) Project 6131 Pacific Ave <br /> 1680 Rogers Avenue Project Number 6131 Pacific Ave 1 Stockton Reported <br /> San Jose CA,95112 Project Manager Nick Sudano 01/25/01 07 54 <br /> MTBE Confirmation by EPA Method 8260A- Quality Control <br /> Sequoia Analytical - Morgan Hill <br /> Reporting Spike Source %REC RPD <br /> Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes <br /> Batch OL18017-EPA 5030B IP/TI <br /> Blank(OL18017-BLK1) Prepared&Analyzed 12/15/00 <br /> Methyl tert-butyl ether ND _ 1 00 ug/l <br /> Surrogate 1,2-Dichloroethane-d4 957 100 957 70-130 <br /> LCS(OL18017-BS1) Prepared&Analyzed 12/15/00 <br /> Methyl tert-butyl ether 910 1 00 ug/) 100 910 70-130 <br /> Surrogate 1,1-Dichloroethane-d4 100 100 100 70-130 <br /> Matrix Spike(OL18017-MSI) Source MJK0759-03 Prepared&Analyzed 12/15/00 <br /> Methyl tert-butyl ether 919 v 1 00 ug/l 100 ND 91 9 70-130 <br /> Surrogate 1,1-Dichloroethane-d4 11 4 100 114 70-130 <br /> Matrix Spike Dup(OL18017-MSD1) Source MJK0759-03 Prepared&Analyzed 12/15/00 <br /> hyl Cert-butyl ether -- -- 9 08 �A l 00 Yug/1 10 0 ND --46-8 70-13D -126- - 25 <br /> ogale 1 2-Dichloroethane-d4 112 100 112 70-130 <br /> �uoia Analytical-Morgan Hill The results in this report apply to the samples analyzed in accordance with the chain o <br /> custody document This analytical report must be reproduced in its entirely <br /> Page 9 of 10 <br />