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Nequola 680 Chesapeake Dnvc mood-Cam CA 94 (415) 364-9233 <br /> 404 N Wiget Lane Walnut Creek,CA 94598 (510) 988 9600 FAX(510)988 %73 <br /> CII Analytical 819 Striker Avenue,Suite 8 Sacramento,CA 95834 (916) 921 9600 FAX(916)921 0100 <br /> Enviros Client Proj ID Shell 6131 Pacific, Stockton Sampled 07/02/97-M 1,270 Perkins Ave Sample Descrlpt SB-4-66 5 Received 07/03/97 L <br /> Sonoma, CA 95476 Matrix SOLID Extracted 07/11/97 <br /> Analysis Method 8015Mod/8020 Analyzed 07/12/97 <br /> r Attention Joe Neely _ __ __ - _ Lab Number_9707310-14 __ _ r_ ___ __ __Reported 07J1PJP7 <br /> DC Batch Number GC071197BTEXEXA- <br /> Instrument ID-GCHP18 <br /> Total Purgeable Petroleum Hydrocarbons (TPPH) with BTEX and MTBE <br /> Analyte Detection Limit Sample Results <br /> — - — -- - mg/Kg--- ---------- ----mg/Ks <br /> TPPH as Gas 1 0 N D <br /> Methyl t-Butyl Ether 0 025 N D <br /> Benzene ... .. .... 0.0050 .... ... .. 00064 <br /> Toluene ... ... 0.0050 .. 0 019 <br /> Ethyl Benzene .. .. 00050 ... 00053 <br /> Xylenes (Total) - -- -- -. 00050 .. 0 032 <br /> Chromatogram Pattern <br /> Surrogates Control Limits % % Recovery <br /> Triflucrotoluene 70 130 82 <br /> 4-Bromofluorobenzene 60 140 103 <br /> rt <br /> Analytes reported as N D were not present above the stated limit of detection <br /> SEQUOIA ANALYTICAL - ELAP 41210 <br /> MI regory <br /> Project Manager Page <br />