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4D Sequoia 680 Chesapeake Drive Redwood City,CA 94063 (650) 364 9600 FAX(650)364-9233 <br /> 404 N Wiget Lane Walnut Creek,CA 94598 (510) 988 9600 FAX(510)988 9673 <br /> Analytical 819 Sinker Avenue,Suite 8 Sacramento,CA 95834 (916) 921 9600 FAX(916)921.0 100 <br /> Blaine Tech Services Client Prod ID Shell Stockton/'971009-G2 Sampled 10/09/97 <br /> 1680 Rogers Avenue Sample Descript MW-2 Received 10/10/97 <br /> San Jose, CA 95112 Matrix LIQUID <br /> i= <br /> Analysis Method EPA 8260 Analyzed 10/14/97 <br />;'-Attention-Fran Thie - Lab Number 97105966-02 Reported 10f161�97 f� <br /> QC Batch Number-MS101497MTBEF3A - <br /> Instrument ID F3 <br /> Oxygenate Compounds (EPA 8260) <br /> Analyte Detection Limit Sample Results <br /> ug/L ug/L <br /> Ethanol <br /> t-Butanol 500 N D <br /> Metyl t-Butyl Ether(MTBE) 100 <br /> 0 N D <br /> DI-Isopropyl Ether(DIPS) 2 0 N D <br /> Ethyl t-Butyl Ether (EfBE) 20 N D <br /> t-Amyl Methyl Ether (TAME) 20 N D <br /> ND <br /> Surrogates Control Limits% % Recovery <br /> 1,2-Dichloroethane-d4 76 114 er <br /> 07 <br /> • <br /> nalytes reported as N D re not present above the stated limit of detection <br /> rEO0O1 L 'CAL <br /> - ELAP #1210 <br /> e enner <br /> rolect Manager <br /> Page 4 <br />