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h <br /> Sequoia 680 Chesapeake Drive Redwood GM CA 94063 (650) 364 9600 FAX(650)364-9233 <br /> 404 N Wiget Lane Walnut Creek,CA 94598 (510) 988 9600 FAX(510)988-9673 <br /> Analytical 819 Striker Avenue,Suite B Sacramento,CA 95834 (916) 921-9600 - FAX(916)921.0100 <br /> Blaine Tech Services" --- - Clieni Proj ID - Shell Stockton/971'009-G2 Sampled 10/09/97 <br /> 1680 Rogers Avenue Sample Descript MW-3 Received 10/10/97 ;; <br />—,= San Jose,-CA 951.12 Matrix LIQUID - 4 <br /> Analysis Method"EPA 8260 —Analyzed Analyzed -10/14/97" 1 <br /> Attention Fran Thie- _ _ Lab Number 9710596-03 _ _ _ _ Reported 101 16j97_ <br /> QC Batch Number-MS101497MTBEF3A - -- -- - -- - - -- -- - - - -... --� -- - - - - -- - <br />-Instrument ID F3 <br /> -oxygenate Compounds(EPA 8260)__- <br /> Analyte Detection Limit Sample Results <br /> ug/L ug/L <br /> Ethanol 500 N D <br /> t-Butanol 100 N D <br /> Metyl t-Butyl Ether (MTBE) 20 N D <br /> Di-Isopropyl Ether (DIPE) 20 N D <br /> Ethyl t-Butyl Ether (ETRE) 20 N D <br /> t-Amyl Methyl Ether (TAME) 20 N D <br /> Surrogates Control Limits% % Recovery <br /> 1,2-Dichloroethane-d4 76 114 110 <br /> - a <br /> Analytes reported as were not present above the stated limit of detection <br /> SEQUO A ]CAL - ELAP #1210 ` <br /> Peggy ner <br /> Rrniart Mananar Page 7 <br />