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Sequoia 660 Chesapeake Drive Redwood City, CA 94063 (650) 364-9600 FAX(650)364-9233 <br /> 404N Wiget Lane Walnut Creek,CA 94598 (510) 988 9600 FAX(510) 988 9673 <br /> Analytical 819 Sinker Avenue,Suite 8 Sacramento,CA 95834 (916) 921-9600 FAX(916)921 0100 <br /> i <br /> Blaine Tech Services Client Proj ID Shell Stockton/971009-G2 - Sampled 10/10/97 ' <br /> 1680 Rogers Avenue Sample Descript MW-4 Received 10/10/97 <br /> San Jose, CA 95112 Matrix LIQUID <br /> Analysis Method EPA 8260 Analyzed 10/14/97 <br /> Attention Fran Thie Lab Number 9710596-04 _ _ _ --Reported_10116197 <br /> OC Batch Number MS1 01 497MTBEF3A <br />,nstrument ID F3 <br /> Oxygenate Compounds (EPA 8260) <br /> Analyte Detection Limit Sample Results <br /> ug/L ug/L <br /> Ethanol 5000 N D <br /> t-Butanol 1000 N D <br /> Metyl t-Butyl Ether (MTBE) ..... . . ..... ... 20 . ......... .. ... . 57 <br /> Di-Isopropyl Ether (DIPE) ... . . .... ... 20 .... ... 21 <br /> Ethyl t-Butyl Ether(ETRE) 20 N D <br /> t-Amyl Methyl Ether(TAME) 20 N D <br /> Surrogates Control Limits % % Recovery <br /> 1,2-Dichloroethane-d4 76 114 107 <br /> i <br /> analytes reported as D were not present above the stated limit of detection <br /> SED I LYTICAL - ELAP #1210 <br /> Legg ginner <br /> 3rolect Manager Page 10 <br />