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Sequoia 680 Chesapeake Drive Redwood GM CA 94063 (650) 364 9600 FAX(650)364 9233 <br /> 404 N Wtget Lane Walnut Creek,CA 94598 (510) 988 9600 FAX(510)988 9673 <br /> Analytical 819 Sinker Avenue,Suite 8 Sacramento,CA 95834 (916) 921 9600 FAX(916)921 0100 <br /> Blaine Tech Services Client Prod ID Shell Stockton/971009-132 Sampled 10/09/97 '; <br /> 1680 Rogers Avenue Sample Descript EB Received 10/10/97 ,, <br /> San Jose, CA 95112 Matrix LIQUID r <br /> Analysis Method EPA 8260 Analyzed 10/14/97 t' <br /> Attention Fran Thie Lab Number 9710596-08 Reported 10116197 <br /> DC Batch Number MS1 01 497MTBEF3A <br /> nstrument ID F3 <br /> Oxygenate Compounds (EPA 8260) <br /> Analyte Detection Limit Sample Results <br /> ug/L. ug/L <br /> Ethanol 500 N D <br /> t-Butanol 100 N D <br /> Metyl t-Butyl Ether (MTBE) 20 N D <br /> Di-Isopropyl Ether (DIPE) 20 N D <br /> Ethyl t-Butyl Ether(ETBE) 20 N D <br /> t-Amyl Methyl Ether (TAME) 20 N D <br /> Surrogates Control Limits % % Recovery <br /> 1,2-Dichloroethane-d4 76 114 111 <br /> a <br /> analytes reported as N D were not present above the stated limit of detection <br /> 3EOUM ALYTICAL - ELAP #1210 <br />'eggy Penner <br />'roject Manager Page 22 <br /> m <br />