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Sequoia 680 Chesapeake Drive Redwood City CA 94063 (415) 364 9600 FAX(415) 364 9233 <br /> Analytical 404 N Wiget Line Walnut Creek CA 9459$ (SIQ) 988 9600 FAX(510)988 9673 <br /> 819 Sinker Avenue,Suite 8 Sacramento, CA 95834 (916) 921 9600 FAX(916)921 0100 <br /> Sugro West, Inc Client Project ID Shell,6131 Pacific Ave,Stockton,CA Sampled Sep 22, 1995 <br /> 1050 Melody lane, Ste 160 Sample Matrix Soil Received Sep 25, 1995 <br /> Roseville, CA 95678 Analysis Method EPA 5030/8015/8020 Reported Oct 10, 1995 <br /> Attention WIII Shipp First Sample # 509-1383 <br /> TOTAL PURGEABLE PETROLEUM HYDROCARBONS with BTEX DISTINCTION <br /> Reporting Sample Sample Sample <br /> Analyte Limit ID I.D. ID <br /> mg/kg 509-1383 509-1384 509-1389 <br /> GE03-46 GE03-49 GE04-49 <br /> Purgeable <br /> Hydrocarbons 10 N D N D N D <br /> Benzene 00050 N D N D N D <br /> Toluene 00050 N D N D N D <br /> Ethyl Benzene 00050 N D N D N D <br /> • Total Xylenes 00050 N D N D N D <br /> Chromatogram Pattern -- -- - <br /> Quality Control Data <br /> Report Limit Multiplication Factor 1 0 1 0 1 0 <br /> Date Analyzed 10/6/95 10/6/95 10/6/95 <br /> Instrument Identification GCHP-1 GCHP-1 GCHP-1 <br /> Surrogate Recovery, % 110 100 102 <br /> (OC Limits = 70-1309'x) <br /> Purgeable Hydrocarbons are quantitated against a fresh gasoline standard <br /> Analytes reported as N D were not detected at or above the reporting limit <br /> SEQUOIA ANALYTICAL, ELAP #1624 <br /> Linda C Schneider <br /> Project Manager <br /> 5091368 FUG <2> <br />