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r <br /> v <br /> '�tL`iIl1L'41 V-'Rr_;C;;;,G:l r ,30tATORY r+VALYSSS <br /> � { TP'HI G TP'-i D ° r';-SC O EDB ICAPII PCB <br /> BTX w 3274 <br /> T? ti T 3015 3020 3014 3240 AES or 3084 <br /> T <br /> CON 3011 8260 3t 4 74 0 <br /> 4 5264 3260 7421 ''"� <br /> 1 ' i <br /> IzSuLEADED <br /> i GAS { <br /> oz � <br /> UiqL GAS X <br /> 4 DIES- I X X k { <br /> L�Ft0SE14E + `{ i X X <br /> ' <br /> 1�s�31 UVK FUEL. 4 X � X X <br /> ` <br /> PR I). X <br /> .OIL � ` <br /> CHLOR. ;{ 1 X 1 <br /> SOLVE`lTS <br /> yOh[COR X � X <br /> X l <br /> LVEVIS <br /> X <br /> 50 X <br /> WAS I�E1 X X <br /> U <br /> � <br /> 5ED OIL X X <br /> Third Edition. Thos TMbl�35 faatdetecti n <br /> designated EPA methods descnd in <br /> fied in EP S Manual',Appendix A-20, <br /> Ali analyses methods are design endations for Initial <br /> ;W 346,are Spec noted below. Refer to the'S R f B LU <br /> 2 3 .Regional Board Staff Recoatm <br /> limiu of motor vehicle fuels (gasoline and dicseF). <br /> Evaluation and Imhesn a iO n below he MCI,STLC- for the wasteao Al o�nd oablc limit [the in question will be accepted, <br /> at <br /> Detection Limits <br /> however laboratory shall utilize the most conservat've metho . <br /> LABORATORY ANALYSES I MI OLOGY: ,030 3015 mod or GG1�4S 3260 <br /> fatal petroleum Hydrocarbon,Gasoline,GGFID 0)�3015 mod or GC1tiiS 3260 <br /> Total Petroleum Hydrocarbon,Diesel, GCli'ID�ID 3024 or GQUS 3260 <br /> TPH-D $enzeae,Toluene,Xylene&Ethyl Benzene, S 3240 <br /> BTX&E GGHSD 3410,G 4 <br /> CL HC Chlorinated Hydrocarbon,7421 or ICP-AES <br /> Total lead,AA 7420, AA GCT IS 3240(DHS-Luft) <br /> TOTAL L7--,%D Ethylene dibromide (DHS-AB 1803ti <br /> EDB h Flame Ioaiz3tia- Detection tion <br /> GC-FID Gas CInductively ,Couple y, Lend,Zinc and Niekei. <br /> Coupled Plasma Atomic Emission Spectrometry 6fl10 or Atomic A corp <br /> ICAP or AA Spectrometry <br /> Chromium 1II and VI,i e <br /> Spectrometry 7000. Metals: Cadmium, <br /> PCB Polychlorinated Biphenyls.GCIMS 3270 or 9030 <br /> ,Method 3050 A=id digestion <br /> 40 Soxhlet sample preparation <br /> Method 35 <br /> Method 3540 Sonication sample preparation,extraction method <br /> Method 5030 Purge and trap sample preparation <br /> re Caa ti of <br /> QAlQC <br /> QuaLity AssurancelQuatiry columns are <br /> column may.be Hied aS a first cut with'dirty'satstvles or once the hydrocarbons <br /> Notes: -TO= false positive detection of benzene, benzene-free solvents are to be used- Faced capillaryhe <br /> - ..... a. asked coseries - --- <br /> --- _._.. _...__._. <br /> preferred to packed columns;roper QA/AC is foFlowcd. <br /> ave been characterized and Q <br /> ur Drinking water saurces,l;PA recommends that the 400 series for volatile organics be used in ptefereace to t <br /> F are lower the QAIQC is better. <br /> �- because the detection limits <br /> Page 3 <br /> Eu 23 043 (Rev 413191) <br />