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Quanferra <br /> Environmental <br /> services <br /> 6X SPIKE/MATRIX SPIKE DUPLICATE QC REPORT <br /> Mt s Analysis and Preparation <br /> Ia <br /> oiect: 096392 <br /> tegory: ICP-AD ICP Metals / Dissolved <br /> im&le <br /> st : ICP-SCAN-6010A-AD Method: 6010A <br /> trix : AQUEOUS <br /> : 096483-0007 <br /> MS un : 10 DEC 97-RD <br /> its mg/L <br /> ---------Concentration--------- Amount Acceptance <br /> Sample MS MSD Spiked %Recovery %RPD Limit <br />'Analyte Result Result Result MS MSD MS MSD Recov. RPD <br /> Aluminum 0.52 2.49 2.46 2.00 2.00 98 97 1 .65 80-120 20 <br /> timony ND 0.490 0.500 0.500 0.500 98 100 2.13 80-120 20 <br /> Fsenic ND 1 .93 1.88 2.00 2.00 97 94 2.61 80-120 20 <br /> arium 0.012 1 .91 1 .84 2.00 2.00 95 91 3.81 80-120 20 <br /> Beryllium ND 0.0460 0.0445 0.0500 0.0500 92 89 3.22 80-120 20 <br /> Iron 1 .3 2.27 2.23 1 .00 1 .00 93 89 4.10 80-120 20 <br /> dmium ND 0.0541 0.0560 0.0500 0.0500 108 112 3.34 80-120 20 <br /> Calcium 408 446 439 50.0 50.0 NC NC NC 80-120 20 <br /> romium ND 0.176 0. 180 0.200 0.200 88 90 2.07 80-120 20 <br /> balt 0.043 0.485 0.478 0.500 0.500 88 87 1.73 80-120 20 <br /> Aper ND 0.236 0.229 0.250 0.250 94 92 3. 10 80-120 20 <br /> Iron 0.023 0.967 0.948 1 .00 1 .00 94 93 2.04 80-120 20 <br /> ND 0.441 0.424 0.500 0.500 88 85 3.82 80-120 20 <br /> loum 0.061 1.07 1 .02 1 .00 1 .00 101 96 5.31 80-120 20 <br /> esium 144 193 187 50.0 50.0 98 87 12.6 80-120 20 <br /> Manganese 0.87 1 .32 1 .29 0.500 0.500 91 85 6.48 80-120 20 <br /> lybdenum ND 0.937 0.922 1 .00 1.00 94 92 1 .58 80-120 20 <br /> Pckel 0.43 0.863 0.842 0.500 0.500 87 83 5.00 80-120 20 <br /> ot ass i um 3.9 51 .9 51 .7 50.0 50.0 96 96 0.36 80-120 20 <br /> 5 lenium ND 1.88 1 .87 2.00 2.00 94 94 0.56 80-120 20 <br /> licon 15.2 24.7 24.2 10.0 10.0 95 90 5.20 80120 20 <br /> � <br /> Iver ND 0.0405 0.0448 0.0500 0.0500 81 90 10. 1 80-120 20 <br /> Sodium 74.0 124 119 50.0 50.0 100 91 9.84 80-120 20 <br /> lfur 516 523 511 10.0 10.0 NC NC NC 0-0 0 <br /> Iallium ND 1 .74 1 .89 2.00 2.00 87 94 7.98 80120 20 <br /> n 0.0066 1 .89 1 .89 2.00 2.00 94 94 0. 17 80-120 20 <br /> Titanium ND 0.959 0.932 1 .00 1.00 96 93 2.77 0-0 0 <br /> nadium ND 0.463 0.453 0.500 0.500 93 91 2.04 80-120 20 <br /> �nc 0.041 0.521 0.516 0.500 0.500 96 95 1 .06 80-120 20 <br /> = Not Calculated, calculation not applicable. <br /> = Not Detected <br /> Caelations are performed before rounding to avoid round-off errors in calculated results. <br />