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'00 . <br /> { <br /> AIR, WATER and HAZARDOUS WASTE LABORATORY CERTIFIED by CALIFORNIA DEPT of HEALTH SERVICES <br /> r <br /> Coast-to- Coast-to-Coast <br /> Coast Lob Number: OSQB@21 <br /> Analytical Services, Inc. Collected: <br /> Analytical 141 Suburban Road , Suite C-4 <br /> Services Son Luis Obispo, California 93401 Tested. <br /> (805) 543-2553 08/®2/97 <br /> Collected by: <br /> FUEL FINGERPRINT ANALYSIS <br /> CAL DHS (TPH Draft) Method & EPA Method 8240/8260-(GC/MS) <br /> Extracted by EPA Method 5039 (purge-bnd-trap) <br /> CCAS-BENICIA SAMPLE DESCRIPTION: <br /> DI Water Spiked to 8.7ppm <br /> with Diesel#2 <br /> i <br /> A Compound Analyzed <br /> PQL Expected Actual Percent <br /> Recovery <br /> ---------------m4/1--- In mg/l in mg/l. <br /> Benzene 0.005 <br /> Toluene <DL not found n/o <br /> 0.005 0.02 0.021 16596 <br /> Ethylbenzeno 9.005 <DL <br /> Xylenes not found 11/0 <br /> 0.095 0.02 6.026 13096 <br /> 1,2-bichloroethane (EDC)) 0.005 n/s not found <br /> Ethylene Dibromide (EDB) 0•x005 n/a <br /> - n/s not found n/a <br /> •yy� ---------------`---`_-•�-_------------ <br /> --_-------------- <br /> f Total Purgeable Petroleum Hydror.;�rbons --------------^-- <br /> (Diesel ##2) 9.5 <br /> 8.7 9.8 113% � . <br /> (Jet Fuel, Stoddard Solvent, Gasoline, <br /> Kerosene, Mineral Spirits) <br /> g. not spiked n/a n/a <br /> i <br /> BTX as a Percent of Total Fuel <br /> s 0 S% <br /> n/a <br /> Percent Surrogate Recoveries i <br /> ............................ ... . 90% 100% <br /> ........_.. ....... <br /> *Practical Quantitation Limit---.-- <br /> Constituents reported as "not found" would have been reported if <br /> presort <br /> at or ohove the listed practical quantitation lim:�t, <br /> Respectfull'y' submitted, <br /> COAST-to-COAS ALY AL SERVICES <br /> �9 <br /> Mary Ha icek, Ph.D. <br /> ... <br /> Incos 508/7 President <br /> QS8021DW.wr1/FFP84 ' <br /> MH/hc/hc <br /> j; <br /> rj <br />