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09/15/97 17:45 `$916 362 0947 SPARGER <br /> 0023/029 <br /> Spalviur <br /> Laborat DMsi°ry on <br /> Tdchno Inc.0AnolykalNle Laboratory DM$Ion <br /> - <br /> Mo <br /> With Automation in Mind Scientific Division <br /> EPA Method 8260 GCMS <br /> Matrix Spike (MS) and Matrix Duplicate Spike (MSD) <br /> Attention: Mr.Jeffrey Rothgery Date Sampled: Jul 29, 1997 <br /> Apex Envirotech, Inc. Date Received: Jul 30, 1997 <br /> 7844 Madison Ave., Ste, 106 Date Analyzed: Aug 10, 1997 <br /> Pair Oaks, CA 95628 Invoice#: 8141 <br /> Project#: ERA02.004 Project Name: Moore Petroleum <br /> 1, Client ID: MSlMSD Batch <br /> LAB ID: 8190-001 MS <br /> 8190-00 i MSD <br /> Matrix: Water Dilution: <br /> UNITS ug/l <br /> Sample Spike MS MSD QC Limits <br /> Compound Conc Added MS MSD %Rec %Rec RPD RPD % Rec <br /> r 1,1-Dichloroethene NO 5000 5119 5517 102% 110% 7.5% 20 61-145 <br /> Benzene 13 5000 5071 5186 101% 1030/a 2.2% 20 76-127 <br /> I <br /> Trichloroethene ND 5000 5119 5301 102% 106% 3.5% 20 71-135 <br /> F <br /> Toluene ND 5000 5075 5270 102% 105% 3.8% 20 76-130 <br /> Chlorobenzere 14 5000 5078 5374 101% 107% 5.7% 20 75-130 <br /> 5 130 <br /> ppb=parts per bi3ion=60-miarogams per Ater <br /> ppm,Porto per milian uglml-mi^Joprams per md!Aer <br /> ND=Not Detected. Contyound(s)maybe presem at concentrations below:hs delecton Ismii. <br /> i ! <br /> i <br /> Aug 12, 1997 <br /> R.L.James,Primpai Chemist Date Reported <br /> SPARGER TECHNOLOGY ANALYTICAL LABORATORY.INC.IS CERTIFIER BY THE STATE OF CALIFORNIA. <br /> DEPARTMENT OF HEALTH SERVICES AS A HAZARDOUS WASTE TESTING LABORATORY <br /> I {Cert�1}7n f:o.161i} <br /> 8260msw <br /> d 3050 Fite Circle Suite 112 9 Sacramento, California 95827 • (916) 362-8947 • FAX(946) 362-0947 <br />