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Spargero Analytical Laboratory Division <br /> Technolo yInc. Mobile Laboratory Division <br /> g Scientific Division <br /> With Automation in Mind <br /> EPA Method 8260 GCMS <br /> Matrix Spike (MS) and Matrix Duplicate Spike (MSD) <br /> Attention: Mr. Tom Landwehr Date Sampled: Jan 26, 2000 <br /> Apex Envirotech Date Received: Jan 27 2000 <br /> p , <br /> 7844 Madison Ave. Ste. 106 Date Analyzed: Jan 28, 2000 <br /> Fair Oaks, CA 95628 Invoice#: 11868JAN00 <br /> Project#: ERA 02.004 Project Name: Moore Petroleum Banta <br /> Client ID: MSIMSD LAB ID: 11868-002MSIMSD <br /> Matrix: Water Dilution: 1: 1 <br /> Units = (uglL) <br /> Sample Spike MS MSD i Limits <br /> Compound Conic Added MS MSD % Rec % Rec RPD RPD % Rec <br /> i <br /> 1,1-Dichloroethene ND 50 66 62 132% 124% 6% 20 61-145 ' <br /> Benzene ND 50 49 45 98% 90% 9% 20 76-127 <br />` Trichloroethene ND 50 46 43 92% 86% 7% 20 71-135 <br /> Toluene ND 50 47 43 94% 86% 9% 20 76-130 <br /> Chlorobenzene ND 50 45 41 90% 82% 9% 20 75-130 <br /> pI <br />` ppb=parts per billion=ug)l=micrograms per liter <br /> ppm=parts per million=uglmi=microgram*per milliliter <br /> ND=Not Detected. Compound(s)may be present at concentrations below the detection limit_ I <br /> k <br /> C <br /> f <br /> Jan 28, 2000 <br /> R. L.James, Principal Chemist Date Reported <br /> U SPARGER TECHNOLOGY ANALYTICAL LABORATORY,INC.IS CERTIFIED BY THE STATE OF CALIFORNIA <br /> DEPARTMENT OF HEALTH SERVICES AS A HAZARDOUS WASTE TESTING LABORATORY <br /> (Certification No.1614) <br /> Oxygenate{W).xls <br /> 3050 Fite Circle, Suite 112 • Sacramento, California 95827 • (996) 362-8947 9 FAX(996) 362-0947 <br />