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819 Striker Avenue,Suite 8 <br /> Sequoia Sacramento, 95834 <br /> (91G)9292 1-9G009600 <br /> FAX(916)921-0100 <br /> Analytical www.secluoialabs.com <br /> Kleinfelder-Stockton Project: Del Monte 5305529 <br /> 2825 East Myrtle Street Project Number: 12280 Reported: <br /> Stockton CA,95205 Project Manager, Joe Zilles 06/04/03 14:07 <br /> Volatile Organic Compounds by EPA Method 8260B - Quality Control <br /> Sequoia Analytical- Sacramento <br /> Reporting Spike Source %REC RPD <br /> Analyte Result Limit Units Level Result %REC Limits APD Limit Notes <br /> Batch 3050503-EPA 5030B (P/TI <br /> Blank(3050503-BLK1) Prepared&Analyzed: 05/29/03 <br /> Tert-butyl alcohol ND 5.0 ug/l <br /> Methyl tort-butyl ether ND LO " <br /> Di-isopropyl ether ND 0.50 " <br /> Ethyl tert-butyl ether ND' 0.50 " <br /> Tert-amyl methyl ether ND 0.50 " <br /> V Ethanol ND 50 " <br /> 1,2-Dichioroethane ND 0.50 " <br /> 1,2-Dibromoethane(EDB) ND 0.50 " <br /> Surrogate:1,2-DCA-d4 14.8 15.0 99 60-140 <br /> Blank(3050503-BLK') Prepared&Analyzed:05/30/03 <br /> ! -t-butyl alcohol ND 5.0 ugA <br /> .ethyl tert-butyl ether ND 1.0 " <br /> Di-isopropyl ether ND 0.50 " <br /> Ethyl tert-butyl ether ND 0.50 <br /> Tert-amyl methyl ether ND 0.50 <br /> Ethanol ND 50 <br /> 1,2-Dichlomethane ND 0.50 " <br /> 1,2-Dibromoethane(EDB) ND 0.50 <br /> Surrogate:1,2-DCA-d4 21.2 25.0 85 60-140 <br /> Laboratory Control Sample(3050503-BSI) _ Prepared&Analyzed: 05/29/03 <br /> Methyl tort-butyl ether 26.2 l.0 ug/l 22.4 117 60-140 <br /> Surrogate:1,2-DCA-d4 17.7 25.-0 111 60-140 — <br /> Laboratory Control Sample(3050503-BS2) Prepared&Analyzed:05/30/03 <br /> Methyl tert-butyl ether 16.4 1.0 - ug/l 22.4 73 60-140 <br /> Surrogate:1,2-DCA44 22.5 25.0 90 60-140 <br /> gtloia Analytical-Sacramento The results in this report apply to the samples analyzed in accordance with the chain of <br /> custody document. This analytical report must be reproduced in its entirety. <br /> Page 8 of 11 <br />