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a Sequoia 680 Chesapeake Drive Redwood City CA 94063 (415) 364.9600 FAX(415) 364-9233 404 N.Wiget Lane Walnut Creek,CA 94598 (510) 988.9600 FAX(510)988-9673 Analytical 819 Striker Avenue,Suite a Sacramento,CA 95834 (916) 921.9600 FAX(916)921-0100 ...�.:.:.....r.....: .......n..v.w:.unv�+.... ..rv.r....+...v.+.:::.+...::...............x.::xN..�. .n..n..n.:.r:.+.:.+.:::::.. �..v.+v.+.::.�.:.�.:::.r:::........-:.'{:.:a.-}. ::h.. ..{M.1..C..L..}.:h.}............0:.{�.{J:U:U:....................h. ...h}....... 4:�K-:�:rv.}{::.. i - ti!!Q.bl'J... ...... ... ... ... . }•.•.rv.•v.} .- ..:.:......x.............:. ....{............:...v.C...........o:f::i:tt*.c!trk.}:ry:. - :.tr::}rnn::fi:}}.{.....:..... >Srnith Environmental Client Project ID: 15674, 94-36901-10 =;N ;3-1260 Graphics Drive Matra: Liquid ±` Y ;;Modesto, CA 95351-1502 aAttentlon: Jeanne Hornsey Work Order#: 9605189 -01-06 Reported: May 13, 1996 ..v...:...::::.+.::..:...x.:..vx.::::::::.v:...+..v.:. ::.:::::...:::. .....................................................::::........ � +..v:.U..::::::d......h.,t:a:}r.:h:"{ao::r:::t:{.}:^:hx^.::or.::%:<h:o:-:{w.-::r:.�:�.,;.•tr{,:;x;;}:;;:<:�i:^'.t<ti<::vtii::?�:?tS;:Y�;v::`:;;,:: „�...... - .:.h:U..C:UC:.x.;{.v.:x ...............:............. ...o.Co: i ....{.....................r.}....n.......n..r rrv...rry.}vr.rvr...r. n n ....... ... QUALITY CONTROL DATA REPORT Analyte: Benzene Toluene Ethyl Xylenes Diesel Benzene QC Batch#: GC050WBTEX17A GC050896BTEX17A GCO50896STEX17A GC050896BTEX17A GCO507960HBPEXZ Analy. Method: EPA 8020 EPA 8020 EPA 8020 EPA 8020 EPA 8015M Prep. Method: EPA 5030 EPA 5030 EPA 5030 EPA 5030 EPA 3520 Analyst: J.Woo J.Woo J.Woo J.Woo J.Minkel MS/MSD#: 96o4K48o1 9604K4601 9604K4801 9604K4801 BLK050796 Sample Conc.: N.D. N.D. N.D. N.D. N.D. Prepared Date: 5/8/96 5/8/96 5/8/96 5/8/96 5/7/96 Analyzed Date: 5/8/96 5/8/96 5/8/96 5/8/96 5/8/96 Instrument I.D.#: GCHP17 GCHP17 GCHP17 GCHP17 GCHP4 Conc. Spiked: 10Ng/L 10pg/L 10pg/L 30pg/1- 1000pg/L Result: 9.7 9.8 9.7 29 760 MS%Recovery: 97 98 97 97 76 Ys Dup. Result: 9.7 9.8 9.6 28 830 MSD% Recov.: 97 98 96 93 83 RPD: 0.0 0.0 1.0 3.5 8.8 RPD Limit: 0-25 0.25 0-25 0-25 0-50 n s-o w o 1 o tf{n r, ,�'' {c{ h h m -c U x,}x e c h'o{{�o r t {r_ h {h o t h'Ur..c.o.}:m.rr.::a:c•.{co.•r.:U{x�'eo::{'i`'}":{:i::';i'.v�..:.a'b"r• -c ..�''�'. ,..,S.�S.?::r.':;ti"v`�'.,ec:o"�":�"'v:� tr'U{};a' vr:'{r:r:'tr:atry:c..v .:d:xor{vx.}.trW.cca}t?w w�Yx*R�.U�ir?�$.+}.:4c:}svti*::�trrtr].trox•:�j,?v:a�:,i:o}?:�.`-cr:r%:i� c.Wo.tr.i.' tr��r��•..rr.n..;..r:: !?}.::0:}:.'f}.:.. x?i{}hwxtr:tr:tr;tr�:!}.,0: ]? .....' 'A:•}:x:tr.tr:»:to}?a^:... +0..o.?v.tr.a*:a u .Cv'i}vi::A'"+.h.:fiJ`::^..C..{!O.v.8:.0+{..3].O:G::-}v.:::Ufk.M::^T'::=^::'.'�C'x':^.�.rf'.C::C:.x�..:.:-trti:C^`^"'i},{h. }3h\'^�?n:$�..'-.::J.`4::'G.•?:f.:..:..:tr:0:]::yitrb:':.:.:}�O)?J'.�:!L'fi:}s`:+....:.......A:...h:}.hfk h.4n0.}0v.�iwnrrxrn-:x:':ttiv`vi�}$...{... LCS#: BLK050896 BLK050896 BLK050996 BLK050896 Not applicable Prepared Date: 5/8/96 5/8/96 5/8/96 5/8/96 Analyzed Date: 5/8/96 5/8/96 5/8/96 5/8/96 Instrument I.D.#: GCHP17 GCHP17 GCHP17 GCHP17 Conc. Spiked: 10pg/L 10pg/L 10pg/L 30,ug/L LCS Result: 9.7 9.7 9.8 29 LCS%Recov.: 97 97 98 97 M 60140 60-140 60-140 60140 50150 LCS 70.130 70-130 70130 70-130 60-140 Control Limits Please Note: The LCS is a control sample of known,interferent-free matrix that is analyzed using the same reagents, .'SEQU91AANAIVTICAL preparation,and analytical methods employed for the samples. The matrix spike is an aliquot of sample fortified with known quantities of specific compounds and subjected to the entire analytical procedure. If the recovery of analytes from the matrix spike does not fall within specified control limits due to matrix interference,the LCS recovery is to be used to validate the batch. Vyt?snsProger **MS=Matrix Spike,MSD=MS Duplicate,FIPD=Relative%Difference 9605189.SSS