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__ ___ <br /> l <br /> SEQUOIA ANALYTICAL <br /> r 880 Chesapeake Drive • Redwood City, CA 94083 <br /> (415) 364-9600 • FAX(415) 364-9233 <br /> U <.: .:::u:: x':xtz:: µ : } N;k• : z0-: <br /> .�.v::v.sw:.:.:.:.:.. ..Au�::r-::::-.,--; �w.:v<:.v-:x{ry•.�+�u+r-.r .-..-.-. .vu.w.v.�n-u.x.:u::.w:.sv-:--0-v ___ <br /> :,'L.4}..-::.:CG3 .v...e.....:..: <br /> ... .::.,.....:.}.....,.,..,,...::.-...:.....fi. .-:.:.:,•::.�}}:3x.:,.-v_,..--x.c:.-_ .,..:r.,�..,.........t.}.ww3 o.{,_,..,......;...,. ...-:.,.:.v....:... - <br /> ..{5:�:-:..:::..:x0-('1,'_=:i-_Yah`_.:a�,.,�:'n";t�W}y.:.u:.t:`:NJ..:V(4:4aW.C'A� - o}r.•:^v,.::.,,:..o. - <br /> .. XOi:.}$i.:.......... s••-• 1.J.�:0.!O'YMf/h.1.0' __ <br /> rRESNA Client PrajectID: OIN0365A2/Stockton, Smith Canal <br /> 1710 Main Street Matrix: Soil <br /> Escalon, CA 95320 <br /> Attention: ,�ohn Lane CC Sample Grou : 3H2O201-10 Re Aug 1 1993 <br /> ;. 6• <br /> :.,.x-:.xx. :,�Y:.Y.u.-:.�. <br /> I%A QUALITY CONTROL DATA REPORT <br /> E -� <br /> r.� i <br /> _.; ANALYTE Ethyl- <br /> '..-:; Benzene Toluene Benzene Xylenes <br /> Method: EPA 8020 EPA 8026 EPA 8020 EPA 8020 <br /> Analyst: E.Cunanan E.Cunanan E.Cunanan E.Cunanan <br /> Conc.Spiked: 6.20 0.20 0.20 0.60 <br /> =3 Units: mg/kg mg/kg m9/k9 m9/kg <br /> LCS Batch#: GSLK080993 GELK0809M GBLK0e0993 GBLK080993 <br /> Date Prepared: 8/9/93 8/9/93 8/9/93 8/9/93 <br /> Date Analyzed: 8/9/93 8/9/93 8/9/93 8/9/93 <br /> Instrument I.D.#: GCHP-6 GCHP-6 GCHP-5 GCHP-6 <br /> LCS % <br /> 'f Recovery: 95 95 100 97 <br /> E - Control Limits: 60-140 60-140 . 60-140 60-140 <br /> •v:.:}::^,.,..{..s.:J.. .{-�[ihl,.{.:.y.rv:.{..,. v:.{n.::..:.:.F.. n -. �..4}:C:1:.s,.. :.. v.,. -'O+f�tr. w:,U,.:C}54.� :.:5__:-^.^.-.� ..+} -(. <br /> :r.�.,v::rN.c:a.a::b::-:;.v,-.,-,�.,-:.�-:;A�:{.:R-r?w„o-a:o.�x•:-'-. ..,,awJo-iG.._�.,-rv„rv. au�a ,.. -:�} � u.r:4:-0.,,,..�..wc�:-�!!-R�:t:n ti.a�noN.t:Z---rnn.Fc. „w..:,�.r.,,r.o.x�:...�:.-.�:;:,w:cc{aa"::?=:.:.:.--'",.�-�-: <br /> MS/MSD <br /> ' Batch#: 3F=105 3HM105 31-12O105 3HM105 <br /> r:='I Date Prepared: 8/9/93 8/9/93 8/9/93 8/9/93 <br /> Date Analyzed: 8/9/93 8/9/93 8/9/93 8/9/93 <br /> Instrument 1.134: GCHP-6 GCHP-6 GCHP-6 GCHP-6 <br /> Matrix Spike <br /> %Recovery: 85 85 85 85 <br /> Matrix Spike <br /> Duplicate% <br /> Recovery: 85 85 85 85 <br /> j Relative% <br /> Difference: 0.0 0.0 0.0 0.6 <br /> SEQUOIA ANALYTICAL Please Note: <br /> The LCS is a control sample of known,interferent free matrix that is analyzed using the same reagents, <br /> preparation and analytical methods employed for the samples. The LCS%recovery data is used for <br /> VIYY(fJf ` validation of sample batch results. Due to matrix effects,the GIC limits for MS/MSD's are advisory only <br /> and are not used to accept or reject batch results. <br /> Vickie Tague <br /> Project Manager 31-120201MAT <7> <br />