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114 2nd Avenue South #07 Pacheco,CA 94553-5566 <br /> IA <br /> McCampbell Analytical Inc Telephone 925-798-1620 Fax 925-798 1622 <br /> h5p I/www mccanNbell cum E mail niaLu meca bell com <br /> • Advanced GeoEnvironinental, Inc Client Project ID Guardmo+Crawford Date Sampled 12/11/02 <br /> 837 Shaw Road Date Received 12/12/02 <br /> Stockton,CA 95215 Client Contact Paul Dotson Date Extracted 12/17/02 <br /> 1Client P O Date Analyzed 12/17/02 <br /> Oxygenated Volatile Organics by P&T and GC/MS* <br /> Fxtrachon Method SW5030B Analytical Method SW8260B Work Order 62t2215 <br /> 1 Lab ID 0212215-OOIB 0212215-0028 0212215-0038 f 0212215-004B <br /> Client ID MWI MW2 MW3 MW4 <br /> Reporting Limit for <br /> 1 Matrix ---W _W I W W--— DF=l <br /> DF 33 1 1 I s W <br /> E---- I <br />' Compound Concentration ug/kg Ag/L <br /> Dnsopropyl ether(RIPE) ND<17 ND ND ND NA 05 <br /> Ethyl tent-butyl ether(ETRE) ND<17 ND ND ND NA 05 <br /> 1 Methyl-t-butyl ether(MTBE) 54 42 ND ND NA 05 <br /> tert-Amyl methyl ether(TAME) ND<17 ND ND ND NA 05 <br /> 1 t-Butyl alcohol(THA) ND<170 ND ND ND NA 5 0 <br /> i <br /> 1,2-Dibromoethane(EDB) ND<17 ND ND ND NA 0 5 <br /> 1 12-Dichloroethane(1,2-DCA) ND<17 ND ND ND NA 0 5 <br /> 1 Surrogate Recoveries (%) <br /> %SS 905 105 108 108 <br /> 1 Comments <br /> *water and vapor samples and all TCLP&SPLP extracts are reported in jig/L,soil/sludge/solid samples in gg/kg, wipe samples in lig/wtpe <br /> product/otllnon-aqueous liquid samples to mg/L <br /> iND means not detected above the reporting limit NIA means analyte not applicable to this analysts <br /> h)lighter than water immiscible sheen/product is present,i)liquid sample that contains greater than—2 vol %sediment,j)sample diluted due to high <br />' organic content <br /> i <br /> 1 <br /> i <br /> 1 <br /> DHS Certification No 1644 Edward Hamilton, Lab Director <br /> 1 <br />