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MINimUM VERIFICATION LABORATORY ANHLYSIS <br /> OXYGEN <br /> 'TANK 'TANK 'TP11-G TPH-I) HTX&E CL HC '1.O'I'AL M'1'H1i ATE$ n��r"t• I'C13 <br /> b CONTENTS 8015 8015 9020 9010 LEAD 8020 (>vrtltt:, ICRP/ 8270 <br /> 9260 9260 9260 9240 7420 926(1 t'tBA,t)tPlt, AFS or 909() <br /> 9260 7421 t(l till, AA <br /> �fnn�l <br /> N'1,M1 <br /> LEADFU)GAS X X X X <br /> UNI,GAS X X X <br /> DIFISFI, X X <br /> KHROSVNE X X X <br /> UNI: FURL X X X X X <br /> 1'14(31.) ()11, X X X <br /> C11 111014, X <br /> SOLVENTS X X <br /> NONCIII,012 X <br /> SOLVENTS X X <br /> WASTE\ <br /> tis)'D 011, X X X X X X X <br /> All antdysis methods aru tho designated I-PA methods described in EPA SW 946,Third Edition. Those mothods not titund in SW 946 are <br /> Npooiliaully noted below. Itel'er to the "SWR(As LUITI'field Manual", Aplwntlix 1)Q3), Table 3-5 on page A20 for minitnuin detection <br /> litrlim lits uttttor v+eldelu IWI (gallolirto and dier4ol), Refer to "Tri-ltagitn al Hoard Staff lteconlmonflationn lin' Initial 1?valuation and <br /> Investigation of UST'a" for the womc and motor oil mininnun dalection limits. Detection Limits that remain below the MCL,STLC or <br /> Allowable Limit of the contaminant In question will he accepted,however laboratory shall utilize the most conservailvo method. <br /> LABORATORY ANALYSES TERMINOLOGY: <br /> TPII.O Total Petroleum tlydrocarlxon,Gusolino,GC/FID(5030)8015 mod or GC/MS 8260 <br /> TPH•D 'Dotal Potrolcum Ilydrnenrlxm,Diosul.(IC/FID(3550),8017 mad or OC/MS 8260 <br /> 13TX&E13unzunc,'foluenc,Xylone&Elltyd Benzeno,OC11'ID 8020 or GUMS 8260 <br /> CL HC Chlodmtod I-lydrocarlwu,GC/HSD 8010,GC/MS 8240 or 8260 <br /> TOTAL LEAD Total lead,AA 7420, AA 7421 or!CP-AFS 6010 <br /> OXYGENATES MTBE,ETBL',TAML,DIPS,&TBA GUMS 8260(Fur MTBE,screen only you may use 8020) <br /> METALS ICAP or AA Inductively Coupled Plasma Atomic Emission Spectrometry 6010 or Atomic Absorption Spectrometry 7000. Metals: <br /> Cadmium.Chromium Ill and Nil,Lend,Zinc and Nickel, <br /> PCA Polychlorinated Biphonyls,GUMS 8270 or 8080 <br /> GC-FID Gas Chromatography,Flano Ionization Detection <br /> Method 3050 Acid digestion <br /> Method 3540 Soxhlet sample preparation <br /> Method 3550 Sonication sample preparation,extraction method <br /> Method 5030 Purge and trap sample preparation <br /> QA/QC Quality Assuruncu/Quality Control <br /> Nolcs: To avoid falso positive detection of lionzeno,benzono-tine solvants are to he tmd. Fused capillary oolumns are prolbrrcd to packed coluninN:n <br /> packed column may be used as a"lirsl out"with"dirty"sumples or once ilia hydrocarbons have town churauterized and proper QA/QC is followed. For <br /> drinking water sources,EPA recommunds that the 500 serios for volatile organic should be used in proleronec to the 600 series because the detection <br /> limits arc lower and the QA/QC is batter, Samples oxhiliting any level of heavy metal contamination may require further analysis.PIIS-Flip <br /> recommends holding those samples until disposal is Indicated. <br /> EH 23 046 (Rovi.wd 05/09/00) <br /> S <br />