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j SEQUOIA ANALYTICAL <br /> 680 Chesapeake Drive a Redwood City, CA 94063 <br />;I (415) 364-9600 FAX (415) 364-9233 h <br /> :RESNA Client Project ID: W4801, PG&E, Stockton Service Center:: <br /> :1710 Main Street Matrbc: Soil <br /> Escalon, CA 95320 = ` <br /> Attention: Lois Frantz QC Sample Group: 3C42201 I Re rted: Mar 1 i 1 <br /> Po 993 <br /> .:..w......,.✓.:;..•.�.c:u+n:.:w}rift.ri;�.o::c%.w.,.w-}..-.c.a::�..,...A..✓.,.:..:..:.{. - .H?.. ..f.. <br /> .:. ....wwwV.v...,w axil.?:.n.:..r.:..vvw}};i4:•fv}iwvu.v::A:' <br /> I 1 <br /> r <br /> QUALITY CONTROL DATA REPORT <br /> i <br /> w � <br /> ANALYTE Total Extractable E <br /> Petroleum <br /> Hydrocarbons <br /> Method: EPA 8015 <br /> Analyst: C.Lee <br /> Concentration <br /> Spiked: 1s <br /> 4 <br /> LCS Batch#: D&Kwiows5 <br /> Date Prepared: 3/10/93 <br /> Date Analyzed 3/10/93 <br /> Instrument I.D.#: GCHP-4 INJ.A p <br /> LCS % <br /> Recovery: 80 <br /> Control Limits: 50-150 <br /> ?4}:Cv.}:f?:4}}:C??{4}}};?:-rv.;?!?nw,?{w.:-:..... ...... a.\v.`h..A.}'\....:}L....\V:q:.NM\}.fi... .?}M'...-.:lA.y.}Y..}:rIXe.Y}•ny}Y{':rny{.{{.}y}::{.:N.r?.:x{ryx:}::{n-rn}: <br /> ....... .:..:.vw:h:-..�n:?r::::::::.::.v::n:::w::v}:•:}i••:x:•}::G•N•:�:.v::::::::,........ ...... ................:::.....:v:.�::-.v v:::r.4::v v::::.�.. .......... :n...:rnC:-�.4.....::e:..":-..:..-..-.. <br /> {4:::?•:::::::::::::.�:::.'v}.}:}}::::�::.:�.....:...:,::•.�::.:::.�..:-ry:::::.:::.}v::•f:..r...ai...................... ..:...:..n.. ...............................n.n......n..,....}. :............:..n.............:.......,}.....x....... <br /> ......................... ,........C.r..................-......:...:....i................::::�::::�:::.�:.:v:,v}:..{.xv:d.,.:v.{..:v...v.v..:{.:v.:,:v:•v:n.:vv::::::.:v.........::.......e--.-:n:..}:::5:•..............................::.-..,...................r•:v.v:.... <br /> . .. ......................,..........n.... .....:.....{......n... n:. ........n............ .....: ......,a::Rw::::-:.v::•::...... .....v}::...r::a:-J.�:}:{vi:�:::=:4}'r}}=: - - :�:Fi--'.-?.-.r...'--.. <br /> {:,..,:...:u:........?.;.??.,?.:<•;}}:;u.::.:..c%•-s�S,,.::.,,-.,�:.:vu,:......,:....,.......,,,:s.�.u.,,. :...:.,..:w:{:,{:sw.,.. ?>.�..,,,,,...•,...v�....h..w3.:w...:,:..s`...:,..,....{,:."...:.a'a:.:.::.:.:,:>csxxx.,:.:r::x•.w:':xuix3;;::c:r:�:?:_:,:,. =...,:,,;;;;i;.:�•i%6::'w?.uow.{{ts.,.,,,•r,.,:.. <br /> MS/MSD <br /> Batch#: D9303-330-01 i <br /> Date Prepared: 3/9/93 <br /> Date Analyzed 3/9/93 i <br /> Instrument I.D.#: GCHP-5 INJ.B i <br /> Matrix Spike " <br /> % Recovery: 16 <br /> Matrix Spike <br /> Duplicate% <br /> Recovery: 6.7 <br /> Relative% <br /> Difference: 29 <br /> i <br /> Please Note: l <br /> The LCS is a control sample of known,interferent free matrix that is analyzed using the same reagents, k <br /> SEQUOIA ANALYTICAL preparation and analytical methods employed for the samples. The LCS%recovery data is used for <br /> vauidation of sample batch results. Due to matrix effects,the OC limits for MS/MSD's are advisory only <br /> and are not used to accept or reject batch results. <br /> �nrie I <br /> roject Manager 3C42201.WAT <3> <br /> i <br />