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Oct 23 2003 11 : 30AM HP LRSr'4.JFT 3330 p- 8 <br /> t[02nd At==ScLfb,4X,Pache�,G4-8;553-5563 <br /> ' McCampbell Analytical Inc. Tetcpboac:925-799-1620 Fix:925-798-1622 <br /> - :MAWW.l ellemn @-mail resin: ❑.eom <br /> Geo-Logic Client Proi mt ID: #03-876;PG&E- Date Sampled: 10/17/03 <br /> Stockton <br /> 1140 5th Avenue Date Received: 10/17/03 <br /> Crockett,CA 44525 ClIclit Coritact: jccl Grcgcr Dat--Ex+a^,„.ted: 1011103 <br /> CLicnt P.O.: Date Analyzed: 1020,-03 <br /> Volatiles Organics+Oxygenates by.P&T and GC/MS(Basic Target List)* <br /> extriction Mecwd: SW5030B Analytical Method: SW826M Wok Onley.0310290 <br /> Lab ID 0310290-OOIA <br /> Client ID P1 (4.51) <br /> Matrix Soil <br /> Compound Concentration* DF 1 - Aroe=r�s <br /> t mr Compound Canctntration s DF !a; <br /> Acetone ND 1.0 1 50 1 tort-Amyl meth 1 ether(TAME) I ND I 1.0 I s.n <br /> Benzcnc I ND + 1.0 1 5.D Bro_mobenzene ND 1.0 5-0 <br /> Brornochloromethane hu t.0 t 5-0 Brorn chlarvmethane ND 1.0 5.0 <br /> Brave ,.. ND 77, 1 1 -' S.0 Nij 1.0 5.0 <br /> 2-B,.i IrK to . 14 NI)c50 1,0 0 t l?u. 1 slcahol(7,_P ND 1.0 , 25 <br /> n-Butyl benzene _ ND 1 1.0 1 5 0 1 sec-Putv3 benzene ND 10 1 5-0 <br /> Lev-Butyl benzeneIND 1 1.0 ! 5.0 Cartrbn Disulfide ND 1.0_ S_0 <br /> Carbon TUrachloride ND 1.0 5.4 Chlorobenzcrro ND 1.0 5.0 <br /> Cnlorouthane ND 1.0 5.0 2-Chloromh l Vinyl Ether ND 1.0 5.0 <br /> - - ND 1.0 5.0 <br /> t •:Ecro`erm � ,1D 0 5.0 Llilcron,etilane <br /> 2-Chlorotoiuerte NP I n c 0 q_r Hl^rc.olacnr AlU _ <br /> Dibromochloromahane ND_ 1.0 5-0 1.2-Dibrom_c-3-chivy^prcmane NA l 0 5.0 <br /> 1,2-Di4rornoethane EDB ND �_1_D 5.0 1 Dibromomethane ND __ 1,0 5.o <br /> 1,2-Dichlorobetlzene ND I 1.0 5A 1,3-Dichlorobenzene ND 1-05.0 <br /> �---- <br /> 1,4-Dichlorobenzcnc ivli 1.0 50 IiicniorodjfIuoromcthanc ND LO 5.0 <br /> E,]-Dirblcrochs5 , , . , L0DN { 5.0 <br /> 1.1-DicWar cxthene --- ND I I 0 50 'cis-1 2-I1ich!orocthrn' ND --- [.0 5.0 <br /> t=3-1,2-131c_hloroethcne T ND 1.0 _ 5.0_ 1,2-Dichloropmpane __ I _ ND 1.0 5.9 <br /> l,3-t)iehloro am - ND l.D 5,0 2,2-Dichloropropane <br /> 1,i-Uicuhmr are ND 1.0 , 5.0 'cis-1,3-Dichtoro o enc ND 1 5.0 <br /> t-,3Lr,s-1,3-Ciehlara ro z ND 5.0 Diisopfopyt ether'DSPI;) NU <br /> F,th�l►+rnze^te ---E --- N-D ---�'9 c.0 E_h a:eT-Jttt*'t,ay _i�T3r,, :rD <br /> 5.0 <br /> Hexachlorubuladiene ND 1 I.0 1 5.0 2-Hexanona i 0 I SO <br /> lodomcthane(Methyl iodide NA l.0 _50 Iso ro [benzene_ ND Lo 5.4 <br /> 4-Isopropyl loluene ND 1.0 _i S.0 Meth -t-bu t ether MTBE) WD1.0 $.0 <br /> :'.ictn knechloride NI) 1-0 j 5.0 1 4-lvl0.hyl-2- entanonc MIRK NU 1.0 5.0 <br /> *kphfticr,c N'D I:D 5.0 n-P ro 1 benzene 1.0 5.0 <br /> S enc ND 1-A_ m? 1,1t'-7 et^chlor Cl nc \D :.Q 5.0 <br /> 1,1,2,2-Tetrachloroethane _ ND 1.0 I 5.0 Tetrachloroclhene ! 7 al g so <br /> Toluene ND SIA 5.0 1,2,3-TTichbrober ane ND _ 1.0 5.0 <br /> 1,2,4-jrichlorobenzene _ ND 1.0 1 5.0 1,1,1-Tnchloracthane ND1.0 5.0 <br /> 1,1 _Trichlo:oetiane 1rD _ i.0 ZYA i Trichloroethene NU 1 1.0 t 5.0 <br /> Trichlarotlurrrner!t.nc ikn- :0 1 S.0 12,3-Tric'.ttocu :v ane 1�D 1.4 5.D <br /> 1.2,4-Trimeth lbenzene ND 1.6 5,0 1,3,5-Triaecthvlt•rztrtr ND <br /> via]Acetate Np 1.0 50 1 Vinyl Chloride _ NA 1.0 5.0 <br /> Xylenes ND I.0 1 50 ' <br /> Surrogate Recoveries(•lo <br /> °�o5S1: 101 iaSS2: I 9G-g <br /> SS3: - _-t- 107 <br /> Co:ztmatts: <br /> •water Wad t,-por samples and all TCLP&SPLP ext,a.cts are c, cd inµP2,set;'a'.Ldgc.'salid samples is 4 .'kg, wipe samples is 0&4ipt, <br /> producdoil/non-aqueous liquid samples in rng(L. <br /> ND means rot detected Al as a the rcpurtius lindt;N,A rn, q3 aa4iym not applicable to this analysis. <br /> 0 surrogate diluted out of range or surTogale coelutes with another peat <br /> h)liglt:cr than water i-nmiscible s1:ieen'proeuct is present;i)Liquid sarnalc that cc)tains grt:ater than-2 vol.ib acdiniont;j)sample diluted due to high <br /> I-OrRAflic content. <br /> DHS Certification No_ 1644 / ` Angela Rydelius,Lab Manager <br />