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OCT 15 2014 <br /> ENVIRONMENTAL HEALTH <br /> DEPARTMENT <br /> CASTLE ANALYTICAL LABORATORY <br /> Environmental Testing Services 2333 Shultie Drive,Atwater,CA 9530'1 Phone: (209)384-2930 <br /> Certificate No.2480 Fax (209)3841507 <br /> Moore Twining Associates,Inc. Client Project ID:2EO9017 Method:SM 5520'C&F <br /> 2527 Fresno Street Lab Reference Number.1205039 Instrument ID:IR SPEC-1 <br /> Fresno,CA 93721 Sample Description:Soil Extracted;05-1412 <br /> Attn:Julio Morales Analyst Clari J.Cone Analyzed:05-14-12 <br /> Matrix Spike ID:1204047-01 S Reported;05-15-12 <br /> QUALITY CONTROL DATA REPORT <br /> ANALYTE OIL&GREASE <br /> Spike Concentration: . 50 <br /> Units: mg/kg <br /> LCS Batch Y.: TRPH5142 <br /> LCS%Recovery: 94% <br /> Control Limits: 80-130% <br /> MS/MSD Batch# TRPH-5142 <br /> MS%Recovery: 91% <br /> MSD%Recovery: 149% <br /> Relative%Difference: 28% <br /> Please Note: <br /> The LCS(Laboratory Check Sample)is a control sample of known,Interferent free matrix that is fortified with representative <br /> analytes and analyzed using the same reagents,preparation and analytical methods employed for the samples. <br /> The LCS%recovery is used for validation of sample match results. Due to matrix effects,the QC limits and recoveries for . <br /> MSIMSMs are advisory only and not used to accept of reject batch results._ <br /> APPROVED BY: <br /> Ja s :Ph7llips/Le oratory oirectoror <br /> n J.Cone/LaboratoryManager <br />