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' ANALYTICAL <br /> BSKLABORATORIES <br /> Ery Rlfenburg Certificate of Analysis <br /> Foothill Engineering ELAP Certificate#1180 <br /> 12793 Paddy Creek Lane Report Issue Date 06/12/2003 <br /> Lodi, CA 95240 <br /> BSK Submission #• 2003051843 <br /> BSK Sample ID #• 327127 <br /> Project ID Project Desc Connell Motor Truck <br /> Submission Comments <br /> Sample Type Solid Date Sampled 05/27/2003 <br /> Sample Description MWID at 75' Time Sampled 1300 <br /> Sample Comments Date Received 05/29/2003 <br /> Organics Prep Analysis <br /> Analyte Method Result Units PQL Dilution DLR Date Date <br /> TPI{as Gasoline EPA 8015(M) ND mg/Kg I 1 1 06/04/03 06/04/03 <br /> Benzene EPA 8020 ND mg/Kg 0 005 1 0 005 06/04/03 06/04/03 <br /> Ethylbenzene EPA 8020 ND mg/Kg 0 005 1 0 005 06/04/03 06/04/03 <br /> Toluene EPA 8020 ND mg/Kg 0 005 1 0 005 06/04/03 06/04/03 <br /> Total Xylenes EPA 8020 ND mg/Kg 0 005 1 0 005 06/04/03 06/04/03 <br /> 1,2-Dibromoethane EPA 8260 ND µg/Kg 50 1 5 06/07/03 06/07/03 <br /> 1,2-DichlOToethane EPA 8260 34 gg/Kg 50 1 5 0 06/07/03 06/07/03 <br /> Di-isopropyl Ether EPA 8260 ND µg/Kg 5 0 1 5 06/07/03 06/07/03 <br /> Ethyl t-Butyl Ether EPA 8260 ND }tg/Kg 50 1 5 06/07/03 06/07/03 <br /> Methyl-t-Butyl Ether EPA 8260 ND gg/Kg 50 1 5 06/07/03 06/07/03 <br /> t-Amyl Methyl Ether EPA 8260 ND gg/Kg 5 0 1 5 06/07/03 06/07/03 <br /> tert-Butyl Alcohol EPA 8260 ND Ag/Kg 50 1 50 06/07/03 06/07/03 <br /> Surrogate <br /> - - - - - - --- - -- - - - -- - - - - - -- - - -- - - - - - -- -- - - - - - - - - -- - - - -- - - <br /> F'luorobenzene EPA 8020 758 %Rec - I NIA 06/04/03 06/04/03 <br /> Toluene-d8 EPA 8260 100 %Ree I N/A 06/07/03 06/07/03 <br /> mg/L Milligrams/Liter(ppm) PQL Practical Quantitation Limit H Analyzed outside of hold time <br /> mg/Kg Milligrams/Kilogram(ppm) DLR Detection Limit for Reporting P Preliminary result <br /> Rg/L Micrograms/Liter(ppb) PQL x Dilution S Suspect result See Cover Letter for comments <br /> µg/Kg Micrograms/Kilogram(ppb) ND None Detected at DLR E Analysis performed by External laboratory <br /> %Rec Percent Recovered(surrogates) See External Laboratory Report attachments <br /> Report Authentication Code I11111111111all 11111all 111111111111111all 11111111111111111111111111111111111111 Page 5 of 20 <br /> 1414 Stanislaus Street Fresno,CA 93706-1623 Phone 559-497-2888,In CA 800-877-8310 Fax 559-485-6935 <br />