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110 2nd Avenue South,#D7,Pacheco,CA 94553-5560 <br /> Inc.McCampbell Analytical, Telephone:925-798-1620 Fax:925-798-1622 <br /> ' 1 ,4Website:WWW.mccampbell.com E-mail:main@mccampbell.com <br /> • Advanced GeoEnvironmental,Inc. Client Project ID: River City Petroleum Date Sampled: 01/18/05 <br /> ' 837 Shaw Road (Connell) Date Received: 01/21/05 <br /> Client Contact: Bill Little Date Extracted: 01/24/05 <br /> Stockton,CA 95215 <br /> ' Client P.O.: Date Analyzed: 01/24/05 <br /> Oxygenated Volatile Organics+EDB and 1,2-DCA by P&T and GC/MS* <br /> ' Extraction Method:SW5030B Analytical Method:SW8260B Work Order:0501265 <br /> Lab ID 0501265-OOIB 0501265-002B <br /> Client ID MW-36 MW-37 <br /> ' Reporting Limit for <br /> Matrix W W DF=1 <br /> DF 5 1 S `,i, <br /> ' Compound Concentration ug/kg µg/L <br /> ' tert-Amyl methyl ether(TAME) ND<2.5 ND NA 0.5 <br /> t-Butyl alcohol(TBA) ND<25 ND NA 5.0 <br /> ' 1,2-Dibromoethane(EDB) ND<2.5 ND NA 0.5 <br /> 1,2-Dichloroethane(1,2-DCA) 140 ND NA 0.5 <br /> ' Diisopropyl ether(DIPE) ND<2.5 ND NA 0.5 <br /> ' Ethyl tert-butyl ether(ETBE) ND<2.5 ND NA 0.5 <br /> Methyl-t-butyl ether(MTBE) ND<2.5 ND NA 0.5 <br /> Surrogate Recoveries(%) <br /> %SS: 99 99 <br /> Comments <br /> *water and vapor samples are reported inµg/L,soil/sludge/solid samples in mg/kg,product/oil/non-aqueous liquid samples and all TCLP&SPLP <br /> extracts are reported in mg/L,wipe samples in pg/wipe. <br /> ND means not detected above the reporting limit;N/A means analyte not applicable to this analysis. <br /> #surrogate diluted out of range or surrogate coelutes with another peak. <br /> h)lighter than water immiscible sheen/product is present;i)liquid sample that contains greater than—1 vol.%sediment;j)sample diluted due to high <br /> organic content/matrix interference;k)reporting limit near,but not identical to our standard reporting limit due to variable Encore sample weight;m) <br /> ' reporting limit raised due to insufficient samp le amount;n results are reported on a dry weight basis; )see attached narrative. <br /> • <br /> ' DHS Certification No. 1644 Angela Rydelius,Lab Manager <br />