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' t 7 t Analytical., t 110 2nd Avenue South,#D7,Pacheco,CA 94553-5560 <br /> MCCampbell nalytical Inc. Telephone:925-798-1620 Fax:925-798-1622 <br /> http://www.mccarr4)beH.com E-mail:rnain@mccarMbell.com <br /> Advanced GeoEnvironmental,Inc. Client Project ID: Connell Motor Truck Date Sampled: 07/09/03 <br /> ' . 837 Shaw Road Sales Date Received: 07/11/03 <br /> ' Client Contact: Bill Littlle Date Extracted: 07/11/03-07/16/03 <br /> Stockton,CA 95215 <br /> Client P.O.: Date Analyzed: 07/11/03-07/16/03 <br /> ' Volatiles Organics+Oxygenates by P&T and GUMS(Basic Target List)* <br /> Extraction Method: SW5030B Analytical Method: SW8260B Work Order:0307177 <br /> Lab ID 0307177-OOIB <br /> ' Client ID MW 1 <br /> Matrix Water <br /> Reporting <br /> Compound Concentration* DF Re <br /> LLii,nit g Compound Concentration* DF ILimit <br /> ' Acetone ND 1.0 5.0 tert-Am 1 methyl ether(TAME) ND 1.0 1 0.5 <br /> Benzene ND 1.0 0.5 Bromobenzene ND -1-0-T 0.5 <br /> Bromochloromethane ND 1.0 0.5 Bromodichloromethane ND 1.0 0.5 <br /> Bromoform ND 1.0 0.5 Bromomethane ND 1.0 0.5 <br /> ' 2-Butanone EK ND 1.0 1.0 t-Butyl alcohol BA ND 1.0 5.0 <br /> n-Butyl benzene ND 1.0 0.5 sec-Butyl benzene ND 1.0 0.5 <br /> tert-Butyl benzene ND 1.0 0.5 Carbon Disulfide ND 1.0 0.5 <br /> Carbon Tetrachloride ND 1.0 0.5 Chlorobenzene ND 1.0 0.5 <br /> Chlordethane ND 1.0 0.5 2-Chloroeth 1 Vinyl Ether ND 1.0 0.5 <br /> Chloroform ND 1.0 0.5 Chloromethane ND 1.0 0.5 <br /> 2-Chlorotoluene ND 1.0 0.5 4-Chlorotoluene ND 1.0 0.5 <br /> Dibromochloromethane ND 1.0 0.5 1,2-Dibromo-3-chloro ro ane ND 1.0 0.5 <br /> ' 1,2-Dibromoethane(EDB) ND 1.0 0.5 Dibromomethane ND 1.0 0.5 <br /> 1,2-Dichlorobenzene ND 1.0 0.5 1,3-Dichlorobenzene ND 1.0 0.5 <br /> 1,4-Dichlorobenzene ND 1.0 0.5 Dichlorodifluoromethane ND 1.0 0.5 <br /> 1,1-Dichloroethane ND 1.0 0.5 1,2-Dichloroethane 1,2-DCA ND 1.0 0.5 <br /> 1,1-Dichloroethene ND 1.0 0.5 cis-1,2-Dichloroethene ND 1.0 0.5 <br /> trans-l,2-Dichloroethene ND 1.0 0.5 1,2-Dichloro ro ane ND 1.0 0.5 <br /> 1,3-Dichloro ro ane ND 1.0 0.5 2,2-1)ichlororo ane ND 1.0 0.5 <br /> ' 1,1-Dichlororoene ND 1.0 0.5 cis-1,3-Dichloro ro ene ND 1.0 0.5 <br /> trans-l,3-Dichloro ropene ND 1.0 0.5 Diiso ro 1 ether IPE ND 1.0 0.51 <br /> Ethylbenzene ND 1.0 0.5 Ethyl tert-butyl 1 ether ETBE ND 1.0 0.5 <br /> Hexachlorobutadiene MMD1.0 <br /> 2-Hexanone ND 1.0 0.5 <br /> ' Iodomethane(Methyl iodide Iso rolbenzene ND 1.0 0.5 <br /> 4-Iso ro 1 toluene Meth 1-t-bu 1 ether TBE ND 1.0 0.5 <br /> Meth leve chloride 4-Meth 1-2- entanone IBK ND 1.0 0.5 <br /> Na hthalene -Pro 1 benzene ND 1.0 0.5 <br /> Styrene ND 1.0 0.5 1,1,1,2-Tetrachloroethane ND 1.0 0.5 <br /> 1,1,2,2-Tetrachloroethane ND 1.0 0.5 Tetrachloroethene ND 1.0 0.5 <br /> Toluene ND I.0 0.5 1,2,3-Trichlorobenzene ND 1.0 0.5 <br /> 1,2,4-Trichlorobenzene ND 1.0 0.5 1,1,1-Trichloroethane ND 1.0 1 0.5 <br /> ' 1,1,2-Trichloroethane ND 1.0 0.5 Trichloroethene ND 1.0 0.5 <br /> Trichlorofluoromethane ND 1.0 0.5 1,2,3-Trichloro roane ND 1.0 E <br /> 1,2,4-Trimeth (benzene ND 1.0 0.5 1,3,5-Trimeth lbenzene ND 1.0 <br /> Vinyl Acetate ND 1.0 5.0 Vinyl Chloride ND 1.0 0.5 <br /> Xylenes ND L 1.0 1 0.5 <br /> Surrogate Recoveries(%) <br /> %SSI: 102 %SS2: 99.7 <br /> ' %SS3; 105 <br /> Comments: <br /> *water and vapor samples and all TCLP&SPLP extracts are reported inµg/L,soil/sludge/solid samples inµg/kg, wipe samples inµg/wipe, <br /> product/oil/non-aqueous liquid samples in mg/L. <br /> ' ND means not detected above the reporting limit;N/A means analyte not applicable to this analysis. <br /> #surrogate diluted out of range or surrogate coelutes with another peak. <br /> ' h)lighter than water immiscible sheen/product is present;i)liquid sample that contains greater than-2 vol.%sediment;j)sample diluted due to high <br /> or anic content. <br /> ' DHS Certification No. 1644 Angela Rydelius,Lab Manager <br />