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' L Analytical <br /> T 110 2nd Avenue South,#D7,Pacheco,CA 94553-5560 <br /> MCCampbell Analytical Inc. Telephone:925-798-1620 Fax:925-798-1622 <br /> http://www.mccanipbeH.com E-mail:main mccampbell.com <br /> Advanced GeoEnvironmental,Inc. Client Project ID: Connell Motor Truck Date Sampled: 07/09/03 <br /> Sales <br /> 837 Shaw Road Date Received: 07/11/03 <br /> ' Client Contact: Bill Littlle Date Extracted: 07/11/03-07/16/03 <br /> Stockton,CA 95215 <br /> Client P.O.: Date Analyzed: 07/11/03-07/16/03 <br /> ' Volatiles Organics+Oxygenates by P&T and GUMS(Basic Target List)* <br /> Extraction Method: SW5030B Analytical Method: SW8260B Work Order:0307177 <br /> Lab ID 0307177-013B <br /> ' Client ID MW 13 <br /> Matrix Water <br /> Compound Concentration* DF ReLp it g Compound Concentration*1 DF RepLortingvrut <br /> Acetone ND<5.5 1.0 5.0 tert-Am I methyl ether(TAME) ND 1.0 0.5 <br /> Benzene ND 1.0 0.5 Bromobenzene ND 1.0 0.5 <br /> Bromochloromethane ND 1.0 0.5 Bromodichloromethane ND 1.0 0.5 <br /> Bromoform ND 1.0 0.5 Bromomethane ND 1.0 0.5 <br /> ' 2-Butanone EK) ND 1.0 1.0 t-Butyl alcohol A ND 1.0 5.0 <br /> n-Butyl benzene ND 1.0 0.5 1 see-Butyl benzene ND 1.0 0.5 <br /> tert-Butyl benzene ND 1.0 0.5 Carbon Disulfide ND 1.0 0.5 <br /> ' Carbon Tetrachloride ND 1.0 0.5 Chlorobenzene ND 1.0 0.5 <br /> Chloroethane ND 1.0 0.5 2-Chloroethyl Vinyl Ether ND 1.0 0.5 <br /> Chloroform ND 1.0 0.5 Chloromethane ND 1.0 0.5 <br /> 2-Chlorotoluene ND 1.0 0.5 4-Chlorotoluene ND 1.0 0.5 <br /> Dibromochloromethane ND 1.0 0.5 1 2-Dibromo-3-chloro ro ane ND 1.0 0.5 <br /> 1,2-Dibromoethane(EDB) ND 1.0 0.5 Dibromomethane ND 1.0 0.5 <br /> 1,2-Dichlorobenzene ND 1.0 0.5 1,3-Dichlorobenzene ND 1.0 0.5 <br /> 1,4-Dichlorobenzene ND 1.0 0.5 Dichlorodifluoromethane ND 1.0 0.5 <br /> 1,1-Dichloroethane ND 1.0 0.5 1,2-Dichloroethane 1,2-DCA 4.5 1.0 0.5 <br /> ' 1,1-Dichloroethene ND 1.0 0.5 cis-1,2-Dichloroethene ND 1.0 0.5 <br /> trans-1,2-Dichloroethene ND 1.0 0.5 1,2-Dichloro roane ND 1.0 0.5 <br /> 1,3-Dichloro ro ane ND 1.0 0.5 1 2,2-Dichloro ro"ane ND 1.0 0.5 <br /> ' 1,1-Dichlororo ene ND 1.0 0.5 1 cis-1,3-Dichlororo ene ND 1.0 0.5 <br /> trans-l,3-Dichlororo ene ND 1.0 0.5 Diiso ro 1 ether(DIPE) ND 1.0 0.5 , <br /> Eth lbenzene ND 1.0 0.5 Ethyl tert-butyl ether ETBE) ND 1.0 0.5 <br /> Hexachlorobutadiene ND 1.0 0.5 2-Hexanone ND 1.0 0.5 <br /> ' Iodomethane(Methyl iodide) ND 1.0 5.0 Isopropylbenzene ND 1.0 0.5 <br /> 4-1sopropyl toluene ND 1.0 0.5 Meth 1-t-butyl ether TBE 2.2 1.0 0.5 <br /> Methylene chloride ND 1.0 0.5 4-Meth 1-2- entanone I13K) ND 1.0 0.5 <br /> Naphthalene ND 1.0 0.5 n-Propyl benzene ND 1.0 0.5 <br /> ' <br /> Styrene ND 1.0 0.5 1,1,1,2-Tetrachloroethane ND 1.0 0.5 <br /> 1,1,2,2-Tetrachloroethane ND 1.0 0.5 Tetrachloroethene ND 1.0 0.5 <br /> Toluene ND 1.0 0.5 1,2,3-Trichlorobenzene ND 1.0 0.5 <br /> 1,2,4-Trichlorobenzene ND 1.0 0.5 1,1,1-Trichloroethane ND 1.0 0.5 <br /> ' 1,1,2-Trichloroethane ND 1.0 0.5 Trichloroethene ND 1.0 0.5 <br /> Trichlorofluoromethane ND 1.0 0.5 1,2,3-Trichlororo ane ND 1.0 0.5 <br /> 1,2,4-Trimeth (benzene ND 1.0 0.5 1,3,5-Trimethlbenzene ND 1.0 0.5 <br /> Vinyl Acetate ND 1.0 5.0 Vinyl Chloride ND 1.0 0.5 <br /> ' <br /> Xylenes ND 1.0 0.5 <br /> Surrogate Recoveries(%) <br /> %SS1: 102 %SS2: 98.1 <br /> ' %SS3: 113 <br /> Comments: <br /> *water and vapor samples and all TCLP&SPLP extracts are reported inµg/L,soil/sludge/solid samples inµg/kg,.wipe samples inµg/wipe, <br /> product/oil/non-aqueous liquid samples in mg/L. <br /> ' ND means not detected above the reporting limit;N/A means analyte not applicable to this analysis. <br /> • #surrogate diluted out of range or surrogate coelutes with another peak. <br /> ' h)lighter than water immiscible sheen/product is present;i)liquid sample that contains greater than-2 vol.%sediment;j)sample diluted due to high <br /> lorganic content. <br /> DHS Certification No. 1644 _Angela Rydelius,Lab Manager <br />