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' McCampbell Analytical Inc. <br /> 711/OT2ndpAven- <br /> South,#D7,Pacheco,CA 94553-5560 <br /> lehone:925-798-1620 Fax:925-798-1622 <br /> w.mccampbell.coIn E-mail:nlaincampbellxom <br /> ' <br /> FAdvanced GeoEnvironmental, IncrContact: <br /> : Connell Motor Truck Date Sampled: 07/09/03 <br /> • <br /> Shaw Road Date Received: 07/11/03 <br /> ' ill Littlle Date Extracted: 07/11/03-07/16/03 <br /> Stockton,CA 95215 <br /> Client P.O.: Date Analyzed: 07/11/03-07/16/03 <br /> ' Volatiles Organics+Oxygenates by P&T and GC/MS(Basic Target List)* <br /> Extraction Method: SW5030B Analytical Method: SW8260B <br /> Work Order:0307177 <br /> Lab ID 0307177-016B <br /> Client ID MW16 <br /> Matrix Water <br /> Compound Concentration* DF Reporting Reporting <br /> Limit Compound Concentration* DF Limit <br /> ' Acetone ND 1.0 5.0 tert-Amyl methyl ether(TAME) ND 1.0 0.5 <br /> Benzene _ ND 1.0 0.5 Bromobenzene ND 1.0 0.5 <br /> Bromochloromethane ND 1.0 0.5 Bromodichloromethane ND 1.0 0.5 <br /> Bromoform ND 1.0 0.5 Bromomethane ND 1.0 0.5 <br /> ' 2-Butanone EK ND 1.0 1.0 t-Bu 1 alcohol(TBA) ND 1.0 5.0 <br /> n-Butyl benzene ND 1.0 0.5 sec-Bu 1 benzene ND 1.0 0.5 <br /> tert-Bu 1 benzene ND 1.0 0.5 Carbon Disulfide ND 1.0 0.5 <br /> ' Carbon Tetrachloride ND 1.0 0.5 Chlorobenzene ND 1.0 0.5 <br /> Chloroethane ND 1.0 0.5 2-Chloroeth 1 Vinyl Ether ND 1.0 0.5 <br /> Chloroform ND 1.0 0.5 Chloromethane ND 1.0 0.5 <br /> 2-Chlorotoluene ND 1.0 0.5 4-Chlor3toluene ND 1.0 0.5 <br /> ' Dibromochloromethane ND 1.0 0.5 1,2-Dibromo-3-chlororo ane ND 1.0 0.5 <br /> 1,2-Dibromoethane DB ND 1.0 0.5 Dibromomethane ND 1.0 0.5 <br /> 1,2-Dichlorobenzene ND 1.0 0.5 1,3-Dichlorobenzene ND 1.0 0.5 <br /> 1,4-Dichlorobenzene ND 1.0 0.5 Dichlorodifluoromethane ND 1.0 0.5 <br /> lie1,1-Dichloroethane ND 1.0 0.5 1,2-Dichloroethane 1,2-DCA 4.2 1.0 0.5 <br /> l,l-Dichloroethene ND 1.0 0.5 cis-1,2-Dichloroethene ND 1.0 0.5 <br /> trans-1,2-Dichloroethene ND 1.0 0.5 1,2-Dichloro ro ane ND 1.0 0.5 <br /> 1,3-Dichloro ro ane ND 1.0 0.5 2,2-Dichloro ro'ane ND 1.0 0.5 <br /> ' 1,1-Dichloro ro ene ND 1.0 0.5 cis-1,3-Dichlororo ene ND 1.0 0.5 <br /> trans-l,3-Dichloro ro ene ND 1.0 0.5 Diiso ro I ether IPE) ND 1.0 0E1.00.5 <br /> 5 .Eth lbenzene ND 1.0 0.5 Eth 1 tert-bu 1 ether ETBE ND Hexachlorobutadiene ND 1.0 0.5 2-Hexanone ND Iodomethane eth 1 iodide) ND 1.0 5.0 Iso ro lbenzene ND 4-Iso ro 1 toluene ND1.0 0.5 Methyl-t-but I ether TBE ND Meth lene chloride ND 1.0 0.5 4-Meth 1-2- entanone MK ND Na hthalene ND 1.0 0.5 n-Pro1 benzene ND S ene ND 1.0 0.5 1,1,1,2-Tetrachloroethane ND 1,1,2,2-Tetrachloroethane ND 1.0 0.5 Tetrachloroethene ND Toluene ND 1.0 0.5 1,2,3-Trichlorobenzene ND <br /> 1,2,4-Trichlorobenzene ND 1.0 0.5 1,1,1-Trichloroethane ND 1.0 0.5 <br /> ' 1,1,2-Trichloroethane ND 1.0 0.5 Trichloroethene ND 1.0 0.5 <br /> Trichlorofluoromethane ND 1.0 0.5 1,2,3-Trichloro ro ane ND 1.0 0.5 <br /> 1,2,4-Trimethibenzene ND 1.0 0.5 1,3,5-Trimeth lbenzene ND 1.0 0.5 <br /> t Vin 1 Acetate ND 1.0 5.0 Vinyl Chloride ND 1.0 0.5 <br /> Xylenes ND 110 1 0.5 <br /> Surrogate Recoveries(%) <br /> %SS1: -- - <br /> 103 %SS2: 99.0 <br /> %SS3: 117 <br /> Comments: <br /> *water and vapor samples and all TCLP&SPLP extracts are reported inµg/L,soil/sludge/solid samples in pg/kg, wipe samples in jig/wipe, <br /> product/oil/non-aqueous liquid samples in mg/L. <br /> ' ND means not detected above the reporting limit;N/A means analyte not applicable to this analysis. <br /> #surrogate diluted out of range or surrogate coelutes with another peak. <br /> ' h)lighter than water immiscible sheen/product is present;i)liquid sample that contains greater than-2 vol.%sediment;j)sample diluted due to high <br /> organic content. <br /> ' DHS Certification No. 1644 _Angela Rydelius,Lab Manager <br />