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' MCCampbell Analytical Inc. 110 2nd Avenue South,#D7,Pacheco,CA 94553-5560 <br /> Telephone:925-798-162o Fax:925-798-1622 <br /> httD://www.mccanipbell.com E-mail:main mccaymbell.com <br /> ' r83 <br /> anced GeoEnvironmental,Inc. Client Project ID: Connell Motor Truck Date Sampled: 07/09/03 <br /> Sales <br /> Shaw Road Date Received: 07/11/03 <br /> tStockton,CA 95215 Client Contact: Bill Littlle Date Extracted: 07/11/03-07/16/03 <br /> Client P.O.: Date Analyzed: 07/11/03-07/16/03 <br /> ' Volatiles Organics+Oxygenates by P&T and GC/MS(Basic Target List)* <br /> [Extraction Method: SW5030B Analytical Method: SW8260B <br /> Work Order.0307177 <br /> Lab ID 0307177-018B <br /> ' Client ID OW1 <br /> Matrix Water <br /> Compound Concentration* DF R �s Compound Concentration* DF Reporting <br /> :-jj .5Acetone 5.0 tert-Am ]methyl ether TAME ND 1.0 0.5Benzene 0.5 Bromobenzene ND 1.0 0.5 <br /> Bromochloromethane 0.5 Bromodichloromethane ND 1.0 0.5 <br /> Bromoform 0.5 Bromomethane ND 1.0 0.5 <br /> 2-Butanone(MEK) 1.0 t-Bu 1 alcohol A ND 1.0 5.0 <br /> n-Butyl benzene 1.0 0.5 sec-Butyl benzene 7.2 1.0 0.5 <br /> tert-Bury.1 benzene 0.64 1.0 0.5 Carbon Disulfide ND 1.0 0.5 <br /> ' Carbon Tetrachloride ND 1.0 0.5 Chlorobenzene 9.1 1.0 0.5 <br /> Chloroethane ND 1.0 0.5 2-Chloroeth l Vinyl Ether ND 1.0 0.5 <br /> Chloroform ND 1.0 0.5 Chloromethane aND <br /> 1.0 0.5 <br /> 2-Chlorotoluene ND 1.0 0.5 4-Chlorotoluene 1.0 0.5 <br /> ' Dibromochloromethane ND 1.0 0.5 1,2-Dibromo-3-chloro ro ane1.0 0.5 <br /> 1,2-Dibromoethane EDB ND 1.0 0.5 Dibromomethane 1.0 0.5 <br /> 1,2-Dichlorobenzene 18 1.0 0.5 1,3-Dichlorobenzene1.0 0.5 <br /> 1,4-Dichlorobenzene 1.4 1.0 0.5 Dichlorodifluoromethane ND 1.0 0.5 <br /> ' <br /> 1,1-Dichloroethane ND 1.0 0.5 1,2-Dichloroethane 1,2-DCA 2.1 1.0 0.5 <br /> I,1-Dichloroethene ND 1.0 0.5 cis-1,2-Dichloroethene ND 1.0 0.5 <br /> trans-l,2-Dichloroethene ND 1.0 0.5 1,2-Dichloro ro ane 0.56 1.0 0.5 <br /> 1,3-Dichloro ro ane ND 1.0 0.5 2,2-Dichloro ro"ane ND 1.0 0.5 <br /> ' 1,1-Dichloro ro ene ND 1.0 0.5 cis-1,3-Dichloro ro ene ND 1.0 0.5 <br /> trans-l,3-Dichloro roene ND 1.0 0.5 Diiso ro1 ether IPE ND 1.0 0.5 , <br /> Eth lbenzene ND 1.0 0.5Eth 1 tert-butyl ether ETBE ND 1.0 0.5 <br /> Hexachlorobutadiene ND 1.0 0.5 2-Hexanone ND 1.0 0.5 <br /> ' Iodomethane(Methyl iodide ND 1.0 5.0 Isppropylbenzene ND 1.0 0.5 <br /> 4-Isopropyl toluene 0.60 1.0 0.5 Meth l-t-but 1 ether(MTBE) ND 1.0 0.5 <br /> Methylene chloride ND 1.0 0.5 4-Meth 1-2- entanone MI3K ND 1.0 0.5 <br /> Naphthalene ND 1.0 0.5 n-Propyl benzene ND 1.0 0.5 <br /> ' S ene ND 1.0 0.5 1,1,1,2-Tetrachloroethane ND 1.0 0.5 <br /> 1,1,2,2-Tetrachloroethane ND 1.0 0.5 Tetrachloroethene ND 1.0 0.5 <br /> Toluene ND 1.0 0.5 1,2,3-Trichlorobenzene ND 1.0 0.5 <br /> 1,2,4-Trichlorobenzene ND' 1.0 0.5 1,1,1-Trichloroethane ND 1.0 0.5 1,1,2-Trichloroethane ND 1.0 0.5 Trichloroethene ND 1.0 0.5 <br /> Trichlorofluoromethane ND 1.0 0.5 1,2,3-Trichlororo ane ND 1.0 0.5 <br /> 1,2,4-Trimeth ]benzene ND 1.0 0.5 1,3,5-Trimeth lbenzene ND 1.0 0.5 <br /> ' <br /> .Vinyl Acetate ND 1.0 5.0 Vinyl Chloride ND 1 1.0 0.5 <br /> Xylenes ND1.0 0.5 <br /> Surrogate Recoveries(%) <br /> %SSI: <br /> 104 %SS2: 99.0 <br /> %SS3: 115 <br /> Comments:i <br /> *water and vapor samples and all TCLP&SPLP extracts are reported in gg/L,soil/sludge/solid samples in pg/kg, wipe samples in gg/wipe, <br /> product/oil/non-aqueous liquid samples in mg/L. <br /> ND means not detected above the reporting limit;N/A means analyte not applicable to this analysis. <br /> •#surrogate diluted out of range or surrogate coelutes with another peak. <br /> h)lighter than water immiscible sheen/product is present;i)liquid sample that contains greater than-2 vol.%sediment;j)sample diluted due to high <br /> organic content. <br /> ' DHS Certification No. 1644 Angela Rydelius, Lab Manager <br />