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00 <br />_ MCCampbell Analytical, InC. <br />"When Conlin, Comets" <br />: w.mmampbelcoed,Phtabnr: made 56$-1701 <br />Web: www.mecampbeg.com E-mail: main@mccmnpbeg.wm <br />Telephone: 877-252-9262 Fax: 925-252-9269 <br />Ponder Environmental Services <br />220 East G Street <br />Benicia, CA 94510 <br />Client Project ID: Tank3302 <br />Date Sampled: <br />01/29/08 <br />Date Received: <br />01/29/08 <br />Client Contact: Jim Ponder <br />Date Extracted: <br />01/29/08 <br />Client P.O.: <br />Date Analyzed <br />01/30/08 <br />CAM / CCR 17 Metals* <br />Lab ID <br />0801699-OOIA <br />Reporting Limit for DF =1; <br />Client ID <br />1701-1 <br />ND means not detected <br />above the reporting limit <br />Matrix <br />S <br />s w <br />Extraction Type <br />FTOTAL <br />mg/Kg mg/L <br />ICP - MS Metals, Concentration* <br />Analytical Method. 6020A Extraction MethodSW3050B <br />Work Order 0801699 <br />Dilution Factor I <br />I 1 <br />Antimony 0.89 <br />0.5 NA <br />Arsenic 9.3 <br />0.5 NA <br />Barium 54 <br />5.0 NA <br />Beryllium ND <br />0.5 NA <br />Cadmium 16 <br />0.25 NA <br />Chromium 63 <br />0.5 NA <br />Cobalt 8.7 <br />0.5 NA <br />Cooper 53 <br />0.5 NA <br />Lead 12 <br />0.5 NA <br />Mercury 2.5 <br />0.05 NA <br />Molybdenum 9.4 <br />0.5 NA <br />Nickel 140 <br />0.5 NA <br />Selenium 1.0 <br />0.5 A <br />Silver ND <br />0.5 NA <br />Thallium ND <br />0.5 NA <br />Vanadium 30 <br />0.5 NA <br />Zinc 62 <br />5.0 NA <br />98 <br />Comments <br />*water samples are reported in µg/1., product/oil/non-aqueous liquid samples and all TCLP / STLC / DISTLC / SPLP extracts are reported in <br />mg/L, soil/sludge/solid samples in mg/kg, wipe samples in pg/wipe, filter samples in lig/filter. <br />p means surrogate diluted out of range; ND means not detected above the reporting limit; N/A means not applicable to this sample or <br />instrument. <br />TOTAL = acid digestion. <br />WET = Waste Extraction Test (STLC). <br />DI WET = Waste Extraction Test using de -ionized water. <br />i) aqueous sample containing greater than -1 vol. % sediment; for DISSOLVED metals, this sample has been preserved prior to filtration; for <br />TOTAL^ metals, a representative sediment -water mixture was digested; I) reporting limit raised due to insufficient sample amount; k) reporting <br />limit raised due to matrix interference; m) estimated value due to low/high surrrogate recovery, caused by matrix interference; n) results are <br />reported on a dry weight basis; p) see attached narrative; 1) "J -Flag" - estimated value detected between the RL & MDL. <br />—�DHS'ELA1"Certific7tion'N"- -.— � AmplaRydelins;-L-ab-Manager <br />