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534 <br />llow <br />' McCampbell Analytical, Inc. : wwwanecampbss Road, E-mail:rg,CA 94565-1701 <br />1;;X. <br />� Web:www.mecampbelLcom E-mmaia(a)mccampbell.com <br />"When Oualim Counts" i Tele bone: 877-252-9262 Fax: 925-252-9269 <br />' QC SUMMARY REPORT FOR SM5520E/F <br />W.O. SarrDle Matrix: Solid QC Matrix: Soil WorkOrder: 0801699 <br />EPA Method SM5520EIF Extraction SM5520EIP <br />BatchlD: 33493 <br />Spiked Sample ID: 0801699.001A <br />Analyte <br />Sample Spiked I MS <br />I MSD MS -MSD LCS <br />LCSD <br />LCS-LCSD Acceptance Criteria (%) <br />mg/Kg mg/Kg e/ Rec. % Rec. % RPD a/ Rec. <br />% Rec. <br />% RPD I MS / MSD RPD LCS/LCSD RPD <br />POG <br />24,000 1000 116 <br />114 0.0791 104 <br />108 <br />4.17 170 - 130 1 30 1 70 - 130 30 <br />All target compounds in the Method Blank of this extraction batch were NO less than the method RL with the following exceptions: <br />NONE <br />BATCH 33493 SUMMARY <br />Sample ID Date Sampled Date Extracted Date Analyzed Sample ID Date Sampled Date Extracted Date Analyzed <br />0801699-OOIA 01/29/08 10:05 AM 01/29/08 01/30/08 5:30 PM <br />> = Matrix Spike; MSD = Matrix Spike Duplicate; LCS = Laboratory Control Sample; LCSD = Laboratory Control Sample Duplicate; RPD = Relative Percent <br />Recovery = 100 - (MS -Sample) / (Amount Spiked); RPD = 100' (MS - MSD) / ((MS + MSD) / 2). <br />contains significant concentrations of analyte relative to the amount spiked, or b) the spiked sample's matrix Interferes with the spike recovery. <br />IIII N/A = not enough sample to perform matrix spike and matrix spike duplicate. <br />INR = analyte concentration in sample exceeds spike amount for soil maids or exceeds 2x spike amount for water matrix or sample diluted due to high matrix or analyte content. <br />DHS ELAP Certification N° 1644 QA/QC Officer <br />