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McCampbell Analytical, Inc. 1534 Willow Pass Road, Pittsburg, main@ 565-1701 <br />+� Web:www.mccempbeg.wm E-mail: mvpQmccampbelLcom <br />Telephone: 877-252-9262 Pax: 925-252-9269 <br />QC SUMMARY REPORT FOR SW8260B <br />W.O. Sample Matrix: Solid QC Matrix: Solid WorkOrder: 0801699 <br />EPA Method SW8260B <br />Extraction SW1311 <br />BatchlD: 33633 <br />Spiked Sample ID: <br />NIA <br />Analyte <br />Sample <br />mg/L <br />Spiked <br />mg/L <br />MS <br />% Rec. <br />MSD <br />% Rec. <br />MS -MSD <br />% RPD <br />LCS <br />% Rec. <br />LCSD <br />% Rec. <br />LCS-LCSD <br />% RPD <br />Acceptance <br />MS / MSD RPD <br />Criteria (%) <br />LCS/LCSD <br />RPD <br />tert-Amyl methyl ether (TAME) <br />NIA <br />0.010 <br />N/A <br />NIA <br />N/A <br />112 <br />113 <br />0.655 <br />N/A <br />N/A <br />70. 130 <br />20 <br />Benzene <br />N/A <br />0.010 <br />NIA <br />N/A <br />N/A <br />111 <br />110 <br />0.805 <br />N/A <br />N/A <br />70 -130 <br />20 <br />t -Butyl alcohol (TBA) <br />NIA <br />0.050 <br />N/A <br />N/A <br />N/A <br />79.9 <br />85.9 <br />7.27 <br />N/A <br />N/A <br />70-130 <br />20 <br />Chlorobenzene <br />N/A <br />0.010 <br />N/A <br />N/A <br />N/A <br />109 <br />Ill <br />1.42 <br />N/A <br />N/A <br />70 -130 <br />20 <br />1,2-Dibromoethane (EDB) <br />N/A <br />0.010 <br />N/A <br />NIA <br />NIA <br />98.8 <br />103 <br />4.34 <br />N/A <br />N/A <br />70- 130 <br />20 <br />1,2-Dichloroethane (1,2 -DCA) <br />N/A <br />0.010 <br />N/A <br />N/A <br />N/A <br />91.6 <br />91.5 <br />0.0573 <br />N/A <br />N/A <br />70- 130 <br />20 <br />1,1-Dichloroethene <br />N/A <br />0.010 <br />N/A <br />N/A <br />N/A <br />1 94.5 <br />103 <br />8.20 <br />1 N/A <br />N/A <br />1 70-130 <br />20 <br />Diisopropyl ether(DIPE) <br />N/A <br />0.010 <br />NIA <br />N/A <br />N/A <br />Ill <br />112 <br />1.15 <br />N/A <br />NIA <br />70- 130 <br />20 <br />Ethyl Cert -butyl ether (ETBE) <br />N/A <br />0.010 <br />N/A <br />N/A <br />N/A <br />106 <br />105 <br />1.27 <br />N/A <br />NIA <br />70- 130 <br />20 <br />Methyl -t -butyl ether (MTBE) <br />N/A <br />0.010 <br />N/A <br />N/A <br />N/A <br />112 <br />112 <br />0 <br />N/A <br />N/A <br />70- 130 <br />20 <br />Toluene <br />N/A <br />0.010 <br />N/A <br />N/A <br />N/A <br />99.4 <br />100 <br />0.946 <br />N/A <br />NIA <br />70 -130 <br />20 <br />Trichloroethene <br />N/A <br />0.010 <br />N/A <br />N/A <br />N/A <br />86.2 <br />86.1 <br />0.143 <br />N/A <br />NIA <br />70-130 <br />20 <br />%SS1: <br />N/A <br />0.010 <br />N/A <br />N/A <br />N/A <br />98 <br />98 <br />0 <br />NIA <br />N/A <br />70 -130 <br />30 <br />%SS2; <br />N/A <br />0.010 <br />N/A <br />N/A <br />N/A <br />100 <br />100 <br />0 <br />N/A <br />N/A <br />70- 130 <br />30 <br />%SS3: <br />N/A <br />1 0.010 <br />1 N/A <br />N/A <br />N/A <br />97 <br />96 <br />1.32 <br />N/A <br />N/A <br />70 -130 <br />30 <br />All target compounds in the Method <br />NONE <br />Blank of this extraction <br />batch were ND less than the method RL with the following <br />exceptions <br />BATCH 33633 SUMMARY <br />Sample ID Date Sampled Date Extracted Date Analyzed Sample ID Date Sampled Date Extracted Date Analyzed <br />0801699-OOIA 01/29/08 10:05 AM 02/05/08 02/11/08 9:41 AM <br />MS = Matrix Spike; MSD = Matrix Spike Duplicate; LCS = Laboratory Control Sample; LCSD = Laboratory Control Sample Uuplicate; RYU = <br />a Recovery = too - (MS -Sample) / (Amount Spiked); RPD = 100' (MS - MSD) / ((MS + MSD) / 2). <br />MF / Msn spike_es&ayer.. a and / nr 2,RPD may fall outside of laboratory acceptance criteria due to one or more of the following reasons: a) the sample is inhomogenous AND <br />contains significant concentrations of analyte relative to the amount spiked, or b) the spiked sample's matrix interferes with the spike recovery. <br />N/A = not enough sample to perform matrix spike and matrix spike duplicate. <br />NR = analyte concentration in sample exceeds spike amount for soil mai or exceeds 2x spike amount for water matrix or sample diluted due to high matrix or analyte content. <br />DHS ELAP Certification No 1644 yr I QA/QC Officer <br />