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McCamnbell Analytical. Inc. 1534 Willow Pass Road,Pittsburg,CA 94565-1701 <br /> Web:www.mecempbell.wro Email:maia@mmmpbell.com <br /> "When Oual&Counts" Tele hone:877-252-9262 Fax:925-252-9269 <br /> NuStar LP Client Project ID: Fertilizer;Stockton Date Sampled: 05/05/08 <br /> Terminal Waste Date Received 05/05/08 <br /> 1100 Willow Pass Road <br /> Client Contact: Dan Thomas Date Extracted 05/05/08 <br /> Pittsburg,CA 94565 Client P.O.: #4501224877 Date Analyzed 05/06/08 <br /> CAM/CCR 17 Metals* <br /> Lab ID 0805110-003A 0805110-004A Repanlvg Limitfor DF=4 <br /> Client lD 29080311-01 29080311-02 No means not detected <br /> above the reporting limit <br /> Matrix S S s W <br /> Extraction Type TOTAL TOTAL mg/Kg mp/L <br /> ICP-MS Metals,Concentration* <br /> Analytical Method: 6020A Extraction Method: SW3050B W.OkQndot, 0805110 <br /> Dilution Factor 1 1 I 1 I <br /> Antimonv 0.50 2.0 0.5 NA <br /> Arsenic 5.2 12 0.5 NA <br /> Barium 150 87 5.0 NA <br /> Beryllium NO NO 0.5 NA <br /> Cadmium NO 0.74 0.25 NA <br /> Chromium 29 110 0.5 NA <br /> Cobalt 7.7 ll 0.5 NA <br /> Copper 28 77 0.5 NA <br /> Lead 21 1 40 0.5 NA <br /> Mercury 0.065 ND 0.05 NA <br /> Molybdenum 2.6 12 0.5 NA <br /> Nickel 31 120 0.5 NA <br /> Selenium NO NO 0.5 NA <br /> Silver NO NO 0.5 NA <br /> Thallium NO ND 0.5 NA <br /> Vanadium 42 4110.5 NA <br /> Zinc 71 '_in 5,0 NA <br /> %uSS: 101 1 101 <br /> Comments <br /> .water samples are reported in pg/L,product/oil/non-aqueous liquid samples and all TCLP/STLC/DISTLC/SPLP extracts are reported in <br /> mg/L,soil/sludge/solid samples in mg/kg,wipe samples in pg/wipe,filter samples in pg/filter. <br /> #means surrogate diluted out of range;ND means not detected above the reporting limit;N/A means not applicable to this sample or <br /> instrument. <br /> TOTAL=acid digestion. <br /> WET=Waste Extraction Test(STLC). <br /> DI WET=Waste Extraction Test using de-ionized water. <br /> i)aqueous sample containing greater than—1 vol.%sediment;for DISSOLVED metals,this sample has been preserved prior to filtration;for <br /> TOTAL metals,a representative sediment-water mixture was digested;I)reporting limit raised due to insufficient sample amount;1)analyte <br /> detected below quantitation limits;k)reporting limit raised due to matrix interference;m)estimated value due to low/high sumcigate recovery, <br /> caused by matrix interference;n results are reported on a dry weight basis see attached narrative. <br /> DHS ELAP Certification NO 1644 "" — Angela Rydelius,Lab Manager <br />