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Roa }�' MCCampbell Analytical, Inc 534 Willow Pass corn Pittsburg, in@mcc5-1701 �-1 Web:www.mccempbell.cOm E-mail:mainQmccampbedcom "When Oualiry Counts" Tele hone:877-252-9262 Fax:925-252-9269 QC SUMMARY REPORT FOR SW8270D W.O.Sample Matrix: Soil QC Matrix: Soil WorkOrder: 0805110 EPA Method SW8270D Extraction SW13111SW3510C BatchlD:35410 Spiked Sample ID: NIA Analyte Sample Spiked MS MSD MS-MSD LCS LCSD LCS-LCSD Acceptance Criteria(%) mg/L mg/L %Rec. %Rec. %RPD %Rec. %Rec. %RPD MS/MSD RPD LCS/LCSD RPD Acenaphthene N/A 0.050 N/A N/A N/A 61.1 61.6 0.814 N/A N/A 30- 130 30 4-Chloro-3-methylphenol N/A 0.10 N/A N/A N/A 71 68.5 3.66 N/A N/A 30- 130 30 2-Chlorophenol N/A 0.10 N/A N/A N/A 74 75.1 1.39 N/A N/A 30- 130 30 1,4-Dichlorobenzene N/A 0.050 N/A N/A N/A 54.3 54.7 0.807 N/A N/A 30- 130 30 2,4-Dinitrotoluene N/A 0.050 N/A N/A N/A 59.8 59.4 0.805 N/A N/A 30- 130 30 4-Nitrophenol N/A 0.10 N/A N/A N/A 91.1 94.5 3.71 N/A N/A 30- 130 30 N-Nitrosodi-n- ro ylamine N/A 0.050 N/A N/A N/A 95.4 96.2 0.825 N/A N/A 30- 130 30 Pentachlorophenol N/A 0.10 N/A N/A N/A 79.2 79.8 0.654 N/A N/A 30- 130 30 Phenol N/A 0.10 N/A N/A N/A 71.8 72 0.285 N/A N/A 30- 130 30 Pyrene N/A 0.050 N/A N/A N/A 60.2 60.5 0.414 N/A N/A 30- 130 30 1,2,4-Trichlorobenzene N/A 0.050 N/A N/A N/A 53.6 52.4 2.38 N/A N/A 30- 130 30 %SSL N/A 5 N/A N/A N/A 84 85 1.40 N/A N/A 30- 130 30 %SS2: N/A 5 N/A N/A N/A 83 85 2.13 N/A N/A 30- 130 30 %SS3: N/A 5 N/A N/A N/A 88 89 0.336 N/A N/A 30- 130 30 %SS4: N/A 5 N/A N/A N/A 71 72 0.955 N/A N/A 30- 130 30 %SS5: N/A 5 N/A N/A N/A 106 108 1.38 N/A N/A 30-130 30 %SS6: N/A 5 N/A N/A N/A 64 64 0 N/A N/A 30- 130 30 All target compounds in the Method Blank of this extraction batch were NO less than the method RL with the following exceptions: NONE BATCH 35410 SUMMARY Lab ID Date Sampled Date Extracted Date Analyzed Lab ID Date Sampled Date Extracted Date Analyzed 0805110-001A 05/05/08 2:00 PM 05/06/08 05/14/08 9:50 AM 10805110-002A 05/05/08 2:00 PM 05/06/08 05/14/08 11:10 AM MS=Matrix Spike;MSD=Matrix Spike Duplicate;LCS is Laboratory Control Sample;LCSD=Laboratory Control Sample Duplicate;RPD=Relative Percent Deviation. %Recovery=100'(MS-Sample)/(Amount Spiked);RPD=100'(MS- MSD)/((MS+MSD)/2). MS/MSD spike recoveries and/or%RPD may fall outside of laboratory acceptance crkeda due to one or more of the following reasons:a)the sample is Inhomogenous AND contains significant concentrations of analyte relative to the amount spiked,or b)the spiked sample's matrix interferes with the spike recovery. N/A=not enough sample to perform matrix spike and matrix spike duplicate. NR=analyte concentration in sample exceeds spike amount for soil matrix or exceeds 2x spike amount for water matrix or sample diluted due to high matrix or analyte content. OHS ELAP Certification No 1644 "lov- QA/QC Officer