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MINIMUM VERIFI AIION LAIIORAIORY ANAI YSIS <br /> TANK I ANK 11,11 U I PI I U III X do F CA, 1IC 1 O3 AL EDA METALS PCD <br /> N CON 1 LN IS 8011 81115 8020 8010 1 LAD ICAP/ 8210 <br /> 8201) 82611 8200 BZ40 7421) 8240 ASS or 8080 <br /> 74421 AA <br /> } n <br /> Ld <br /> bey � X <br /> ' Dr' by UNL QAS X X <br /> �r <br /> DIOSEL x X <br /> ' KEROSENE. x x <br /> UNK FUEL x x x x x <br /> ' Pitol) oil' X X <br /> CI ILOIt <br /> ' SOLVEN IS X x <br /> NUNCI ILOR <br /> SULVf3N Is x x x <br /> ' WAS 11!1 <br /> USED Ott x x x x X x <br /> ' All auelyses methods ■re designated EPA melhotts descrlbed In CPA SW 846, -1111rd edition 'Inose methods no! found <br /> In S W 846, are specifically noted below Refer 10 the 'SWRCII 1.0171 rleld Manual', Appendix A-20, 1 able 3-5 for <br /> delecllon 11111113 of motor vehicle furls (gasoline and diesel) Refer to 1 2 3 'Itegfonal lloard Staff Recommendations for . ) <br /> W <br /> 11111RI HY11111a11ort and lrtvesligallon of US IT for Ile waste and ntolor oil delccllott Iltnils, <br /> lelectiozr 11111119 Ilrn1 remain 1►tluw the hI( I, SII ( or Allowable IJnll of the coulanduarll Itt gllesllolt will be accep(ed, <br /> hutvevtr Inboralorl shell utilize the mull corrservelive method, <br /> ' 1 AIIORA I OILY ANALYSES I ERNIIN01,00y: <br /> IPI1 0 1elat Petroleum I)ydrocasbon, Oasolinc, OCIFID (5030) 8015 mod or OC/MS 8260 <br /> 1 Pit 1) blot Pelrolcunl I lydr(lcarinln, Diesel, 00FID (3550), 8015 tnod or 0Cm1S 8260 <br /> ' I)Ix & L Ilenune, lolucne, Xylene dr f+lhyl Ilerl7kne, OCRID 8020 or OC/MS 8260 <br /> CL I IC Chlllrinaled I lydnxc,rbon, OCA ISO 81110, OC/MS 8240 <br /> 10 1 AL L A13 total lead, AA 7420, AA 7421 or ICP ALS 6010 <br /> ' C1)n Ethylene dibronlide (DI IS All 1801), ODMS 8240 (DI IS LUF 1) <br /> OC F1D Das Chronlnlography, Flame lonhatlon Imectlon <br /> ICAC or AA Inductively Coupled Plasma Atomic Emission Spectrometry 6010 or Alontie Absorption <br /> Speclrontelry 70110 Metals, Cadtulunl, 1-hronttum 111 and VI, Lead, Llne and Nickel <br /> PCI( Polychitlrinated Ellphenyls, OC/MS 8270 or 8080 <br /> Melluld 3050 Acid digeslion <br /> Melhod 3541) Soxhlct sample preparation <br /> Method 3550 Sonicallon sa1ni11c ptcparallon, exiiaLlion ntclhod <br /> Method 1030 Purge end trap sample preparation <br /> OA/QC Quality Assurance/Quality Control <br /> Holes: 10 avold false positive detection of benzene, bcnune free solvents are to he used [used capillary columns arc <br /> preferred to packed columns, a packed column may be used as a "llrsl cul' with 'dirty' samples or once the hydrocarbons <br /> have been characterized and proper QA/AC Is ft111owcd <br /> ror Drinking water sources, GPA reulntmcnds that Ilse SW serles for volatile organit3 be used In preference to the 6(X1 <br /> series because the detection limits are lower end the QA/QC Is better Samples exhlbilln6 any level of heavy metal <br /> mlandnallon may require further analysis PI IS-E111) rewnu11ends holding these samples until disposal Is Indicated <br /> Ell 23 0,18 (ItcAssed 7/10/92) Page 8 <br />