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' Entech Analytical Labs anta Glara, CA <br /> yt Inc.,, <br /> ' Lab Report No.: H3021709 Date: 02127/2003 Page: 1 <br /> ' Project Name: VALLEY WHOLESALE Analysis; Volatile Organic Compounds by GC/MS Fuel <br /> Project No: 989.2 Method: 8260FA <br /> Prep Meth: SW5030B <br /> ' Field ID: MW-1 Lab Samp ID: 33384-010 <br /> Descr/Location: MWA Recd Date: 0211912003 <br /> Sample Date: 02/1412003 Prep Date: 02/21/2003 <br /> ' Sample Time: 1600 Analysis Date: 02/21/2003 <br /> Matrix: Water QC Batch: WMS11945 <br /> Basis: Not Filtered Notes: <br /> ' Analyte Det Limit Rep Limit Note Result Units Pvc Dil <br /> Methyl-tent-butyl ether(MTBE) 0.3 1. PQL 1.2 UGIL 1 <br /> Ethyl tent-butyl ether(ETBE) 0.5 5. PQL ND UGIL 1 <br /> tent-Amyl methyl ether(TAME) 0.3 5. PQL ND UGIL 1 <br /> Di-isopropyl ether(DIPE) 0.5 5. PQL ND UGIL 1 <br /> tert-Butyl alcohol (TBA) 4.6 10. PQL ND UGIL 1 <br /> 1,2-Dichioroethane 0.3 5. PQL ND UGIL 1 <br /> 1,2-Dibromoethane 0.5 5. PQL ND UGIL 1 <br /> ' SURROGATE AND INTERNAL STANDARD RECOVERIES: <br /> 4-Bromofluorobenzene 65-135 SMEA 102% 1 <br /> Toluene-d8 77-150 SMEA 103% 1 <br /> Dibromotluoromethane 57-156 SMEAAZ 6.8% I 1 <br /> AZ: Surr. recovery outside of acceptance limits due to matrix intert. <br /> 1 <br /> r <br /> 1 <br /> r <br /> r <br /> r <br /> r <br /> Approved by: U""/ Date: <br /> 1 <br />