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1 i <br /> Entech Analytical Labs, Inc., Santa Clara, CA <br /> Lab Report No.: H2112012 Date: 12104/2002 Page: 6 <br /> ' Project Name: VALLEY WHOLESALE Analysis. Volatile Organic Compounds by GC/MS Fuel <br /> Project No: 989.2 Method: 8260FA <br /> Prep Meth: SW5030B <br /> ' Field ID: MW-5 Lab Samp ID: 32205-006 <br /> Deser/L.ocation: MW-5 Recd Date: 11/2212002 <br /> Sample Date: 11/19/2002 Prep Date: 12102!2002 <br /> ' Sample Time: 1411 Analysis Date: 12/02/2002 <br /> Matrix: Water QC Batch: WMS21822 <br /> Basis: Not Filtered Notes: <br /> Analyte Det Limit Rep Limit Note Result Units Pvc Dil <br /> Methyl-tent-butyl ether(MTBE) 0.3 1. PQL 2a UGIL. 1 <br /> ' Ethyl tert-butyl ether(ETBE) 0.5 5. PQL NO UG/L 1 <br /> tert-Amyl methyl ether(TAME) 1 0.3 5. PQL ND UGIL 1 <br /> Di-isopropyl ether(DIPS) 0.5 5. PQL ND UGIL 1 <br /> ' tert-Butyl alcohol (TBA) 4.6 10. PQL NO UGIL 1 <br /> 1,2-Dichloroethane 0.3 5. PQL ND UG/L 1 <br /> 1,2-Dibromoethane 0.5 5. PQL ND UG/L 1 <br /> SURROGATE AND INTERNAL STANDARD RECOVERIES: <br /> ' 4-Bromofluorobenzene 65.135 SMEA 97.9% 1 <br /> Toluene-d8 77-150 SMEA 105.9% 1 <br /> Di bromofluoromethane 57-156 SMEAAZ 14.8% 1 1 <br /> AZ: Surr. recovery outside of acceptance limits due to matrix interf. <br /> Approved by: Date: 67— <br />