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Entech Analytical Labs, Inc., Santa Clara, CA <br /> Lab Report No.: H2112012 Date: 1210412002 page: 9 <br /> Project Name: VALLEY WHOLESALE Analysis: Votatile Organic Compounds by GC/MS Fuel <br /> ' Project No: 989.2 Method: 8260FA <br /> Prep Meth: SW5030B <br /> ' Field ID: MW-8 Lab Samp ID: 32205-009 <br /> Descr/Location: MW-8 Recd Date: 11/22/2002 <br /> Sample Date: 11/19/2002 Prep Date: 12/02/2002 <br /> ' Sample Time: 1541 Analysis Date: 1210212002 <br /> Matrix: Water QC Batch: WMS21822 <br /> Basis: Not Filtered Notes: <br /> Analyte Det Limit Rep Limit Note Result Units Pvc Dil <br /> Methyl-tent-butyl ether(MTBE) 0.3 1. PQL 25. UG/I_ 1 <br /> ' Ethyl tert-butyl ether(ETRE) 0.5 5. PQL ND UGIL 1 <br /> tert-Amyl methyl ether(TAME) 0.3 5. PQL ND UG/L. 1 <br /> DI-isopropyl ether(DIPE) 0.5 5. PQL ND UG/L 1 <br /> tert-Butyl alcohol (TBA) 4.6 10. PQL ND UG/L 1 <br /> 1,2-Dichloroethane 0.3 5. PQL ND UG/L 1 <br /> 1,2-Dibromoethane 0.5 5. PQL ND UG/L 1 <br /> SURROGATE AND INTERNAL STANDARD RECOVERIES: <br /> 4-Bromofluorobenzene 65.135 SMEA 100.3% 1 <br /> Toluene-d8 77-150 SMEA 103.5% 1 <br /> Dibromofluoromethane 57-156 SMEAAZ 10.6% ! 1 <br /> AZ: Surr. recovery outside of acceptance limits due to matrix interf. <br /> 1 <br /> Approved by,'.* Date; 12,1 A0, <br />