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Entech Analytical Labs, Inc., Santa Clara, CA <br /> Lab Report No.: H2082605 Date: 09/05/2002 Page: 1 <br /> Project Name: VALLEY WHOLESALE Analysis: Volatile Organic Compounds by GCIMS Fuel <br /> Project No: 429409E Method: 8260FA <br /> Prep Meth: SW5030B <br /> Field ID: MW-101 Lab Samp ID. 31020-001 <br /> Deser/Location: MW-101 Recd Date: 08/26/2002 <br /> Sample Date: 08/2212002 Prep Date: 08/2812002 <br /> ' Sample Time. 10440 Analysis Date: 08/28/2002 <br /> Matrix: Water QC Batch: WMS21686 <br /> Basis: Not Filtered Notes: <br /> Analyte Det Limit Rep Limit Note Result Units Pvc Dil <br /> Methyl-tert-butyl ether(MTBE) 0.3 5. PQL ND UGIL 1 <br /> Ethyl tent-butyl ether(ETRE) 0.5 5. PQL ND UGIL 1 <br /> tert-Amyl methyl ether(TAME) 0.3 5. PQL ND UGIL 1 <br /> Di-isopropyl ether(DIPS) 0.5 5. PQL ND UGIL 1 <br /> ' tert-Butyl alcohol (TBA) 11. 20. PQL ND UGIL 1 <br /> 1,2-Dichloroethane 0.3 5. PQL ND UGIL 1 <br /> 1,2-Dibromoethane 0.5 5. PQL ND UGIL 1 <br /> ' SURROGATE AND INTERNAL STANDARD RECOVERIES: <br /> 4-Bromofiuorobenzene 65-135 SMSA 95.8% 1 <br /> Toluene-d8 77-150 SMEA 88.4% 1 <br /> Dibromof}uornmethane 57-156 SMEA 100.2% 1 <br /> i <br /> ' Approved by: "(Ve Date: .— <br /> i <br />