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Entech Analytical Labs, Inc., Santa Clara, CA <br /> Lab Report No_: H2O61906 Date: 07/01/2002 Page: 5 <br /> Project Name: VALLEY WHOLESALE Analysis: Volatile Organic Compounds by GC/MS Fuel <br /> Project No: 989.2 Method: 8260FA <br /> Prep Meth: SW5030B <br /> ' Field ID: MW-5 Lab Samp ID: 30380-002 <br /> Descr/Location: MW-5 Recd Date: 06/20/2002 <br /> t Sample Date: 06/18/2002 Prep Date: 06/24/2002 <br /> Sample Time: 1310 Analysis Date: 06/24/2002 <br /> Matrix: Water QC Batch: WMS31610 <br /> Basis: Not Filtered Notes: <br /> ' Analyte Det Limit Rep Limit Note Result Units Pvc Dil <br /> Methyl-tert-butyl ether(MTBE) 0.3 5. PQL 30. UG/L 1 <br /> ' Ethyl tent-butyl ether(ETBE) 0.5 5. PQL ND UG/L 1 <br /> tert-Amyl methyl ether(TAME) 0.3 5. PQL ND UG/L 1 <br /> Di-isopropyl ether(DIPS) 0.5 5. PQL ND UGIL 1 <br /> ' tert-Butyl alcohol (TBA) 11. 20. PQL ND UGIL 1 <br /> 1,2-Dichloroethane 0.3 5. PQL ND UGIL 1 <br /> 1,2-1)ibromoethane 1 0.5 5. PQL ND UGIL 1 <br /> ' SURROGATE AND INTERNAL STANDARD RECOVERIES: <br /> 4-Bromofluorobenzene 65-135 SMEA 104.0° 1 <br /> Toluene-d8 77-150 SMEA 109.0% 1 <br /> Dibromofluoromethane 57-156 SMEA 102.0% 1 <br /> 1 <br /> Approved Dy: vale: 6Z— <br />