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S CASTLE ANALYTICAL LABORATORY <br /> Environmental Testing Services 2333 Shuttle Drive,Atwater, CA 95301 Phone: (209)384-2930 <br /> Certifrcate#2480 Fax: (209)384-1507 <br /> Advanced GeoEnvironmental, Inc. Client Project ID:Grewals Market Sampled:See Below <br /> ' of Northern California Reference Number:4392 Received:01-29-02 <br /> 837 Shaw Road Sample Description:Soil Extracted:01-29-02 <br /> Stockton, CA 95215 Sample Prep/Analysis Method:EPA 5030/8015B, 8020 Analyzed:01-30-02 <br />( Attn: Tim Cuellar <br /> Lab Numbers:4392-125, 13S, 155, 16S, 17S Reported:02-08-02 <br /> TOTAL PETROLEUM HYDROCARBONS -GASOLINE <br /> ' WITH BTEX DISTINCTION <br /> i <br /> I <br /> ' ANALYTE REPORTING LIMIT SAMPLE ID SAMPLE ID SAMPLE ID SAMPLE ID SAMPLE ID <br /> P-11 /45' P-11 160' P-11 180' P-11 190' P-12120' <br /> (mg/kg) (mg/kg) (mg/kg) (mgik9) (mg/kg) (mg/kg) <br /> MTBE 0.010 0.071 NO NO NO NO <br /> BENZENE 0.0050 0.031 NO NO NO NO <br /> ' TOLUENE 0.0050 NO NO NO NO NO <br /> ETHYLBENZENE 0.0050 0.016 NO ND NO NO <br /> TOTAL XYLENES 0.0050 0.038 NO NO NO NO <br /> GASOLINE RANGE <br /> HYDROCARBONS 1,0 NO NO NO NO NO <br /> ' Report Limit Multiplication Factor: <br /> 7 1 7 1 1 <br /> Date Sampled: 01-24-02 01-24-02 01-24-02 01-24-02 01-23-02 <br /> ' Surrogate%Recovery: RD:75.5%1 RD:75.9% FI0:69.7%IAID:70.0% Fro:85.2%I PID;68.0% FID;62.4%1PIDA3.0% Fib:758%I RD:75.3% <br /> Instrument ID: VAR-GC1 VAR-GC1 VAR-GC1 VAR-GC1 VAR-GC1 <br />' Analytes reported as NO were not detected or below the Practical Quantitation Limit <br /> Practical Quantitation Limit W Reporting Limit x Report Limit Multiplication Factor <br />' ANALYST: APPROVED BY: <br /> C!a NCorsa rol�oratol <br /> .Phillips <br /> Director <br />