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i <br /> Analytical Data <br /> Client: SECOR International, Inc. Job Number: 720-7714-1 <br /> Client Sample ID: TP-8' <br /> Lab Sample ID: 720-7714-6 Date Sampled: 02/12/2007 1535 <br /> Client Matrix: Solid Date Received: 02/12/2007 1720 <br /> 8260B Volatile Organic Compounds by GC/MS <br /> Method: 8260B Analysis Batch: 720-18250 Instrument ID: Varian 3900A <br /> Preparation: 5030B Prep Batch: 720-18249 Lab File ID: c:\saturnws\data\200702\02 <br /> Dilution: 200 Initial Weight/Volume: 5.06 g <br /> Date Analyzed: 02/14/2007 0259 Final Weight/Volume: 10 mL <br /> Date Prepared: 02/13/2007 0945 <br /> _Analyte_� DryWt Corrected: N Result(mg/Kg) Qualifier _RL_„ Benzene ND �...�_.�. .-..__.�_....._.—. 0.99 <br /> Ethylbenzene ND 0.99 <br /> Toluene ND 0.99 <br /> MTBE ND 0.99 <br /> Xylenes,Total ND 2.0 <br /> Gasoline Range Organics(GRO)-C5-C12 340 49 <br /> Surrogate_ %Rec Acceptance Limits <br /> LToluene-d8(Burr)__-- 95 50-130 <br /> 1,2-Dichloroethane-d4 <br /> 0-1301,2-Dichloroethane-d4(Surr) 103 60- 140 <br /> + STL San Francisco Page 10 of 21 <br />