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i Report Number 40680 QC Report Matrix Spike!Matrix Spike Duplicate Date 07/17/2006 Project Name Ace Tomato Project Number Duplicate Spiked Duplicate Spiked Spiked Sample RelativeSpike Spiked Spiked Sample Sample RSapeauele Spike elative Percent Percent Parameter mlSample oevl ueleaule Analysis neoteovtcent Rtv ValSample Units MehodAa zed Percent Percent Dlffm mit TPH as Diesel 40680-02 <1 0 200 200 158 166 mg/Kg M EPA 8015 10/26/04 790 829 487 60-140 25 TPH as Diesel Blank <50 1000 1000 927 998 ug/L M EPA 8015 10/26/04 927 998 737 70-130 25 I Benzene 40704-17 <0 0050 00398 00391 00406 00400 mg/Kg EPA 8260B 10/26/04 102 102 0 138 70-130 25 Toluene 40704-17 <0 0050 00398 00391 00377 00374 mg/Kg EPA 8260B 10/26/04 94 8 955 0 748 70-130 25 Tert-Butanol 40704-17 <0 0050 0199 0 196 0185 0180 mg/Kg EPA 8260B 10/26/04 930 91 9 126 70-130 25 Methyl-t-Butyl Ether 40704-17 <0 0050 00398 00391 00364 00365 mg/Kg EPA 8260B 10/26/04 916 932 1 79 70-130 25 Benzene 40735-01 <0 50 400 400 412 384 ug/L EPA 8260B 10/27/04 103 959 704 70-130 25 Toluene 40735-01 <0 50 400 400 428 39 8 ug/L EPA 8260B 10/27/04 107 996 716 70-130 25 Tert-Butanol 40735-01 <5 0 200 200 199 188 ug/L EPA 8260B 10/27104 994 941 552 70-130 25 Methyl-t-Butyl Ether 40735-01 <0 50 400 400 429 403 ug/L EPA 82608 10/27/04 107 101 643 70-130 25 Benzene 40676-02 <0 50 400 400 406 397 ug/L EPA 8260B 10/27/04 101 992 226 70-130 25 Toluene 40676-02 <0 50 400 400 393 386 ug/L EPA 8260B 10/27/04 984 96 5 194 70-130 25 Tert-Butanol 40676-02 <5 0 200 200 193 196 ug/L EPA 8260B 10/27/04 966 978 1 16 70-130 25 Methyl-t-Butyl Ether 40676-02 60 400 400 109 108 ug/L EPA 8260B 10/27/04 121 118 2 94 70-130 25 &q, -- t KIFF ANALYTICAL, LLC Approved By Joe iff 2795 2nd St, Suite 300 Davis, CA 95616 530-297-4800