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i <br /> Alpha Analytical, Inc. - <br /> Q 255 Glendale Ave. • Suite 21 • Sparks, Nevada 89431 -5778 <br /> (775) 355- 1044 • (775) 355-0406 FAX • 1 -800-283- 1183 <br /> Date: Work Order: <br /> 18-Mar- 13 QC Summary Report 13031445 <br /> Method Blank Type: MBLK Test Code: EPA Method SW0260B <br /> File ID: 13031506,D Batch ID: MS09W0315A Analysis Dale: 03115/2013 11 :08 <br /> Sample ID: MBLK MS09W0315A Units : pg/L Run ID: MSD_09_130315A Prep Date: 03/151201311 :08 <br /> Analyte Result PQL SpkVal SpkRefVal %REC LCL(ME) UCL(ME) RPDRefVal %RPD(Limit) Qual <br /> Benzene ND 0.5 <br /> Toluene ND 0.5 <br /> Ethylbenzene ND 0.5 <br /> m ,p-Xylene ND 0.5 <br /> o-Xylene ND 0.5 <br /> Surr: 1 ,2-Dichloroethane-d4 8.23 10 82 70 130 <br /> Surr: TolueneEB 11 . 1 10 111 70 130 <br /> Surr: 4-Bromofluorobenzene 10. 1 10 101 70 130 <br /> Laboratory Control Spike Type: LCS Test Code: EPA Method SW8260B <br /> File ID: 13031504.13 Batch ID: MS09W0315A Analysis Date: 031151201310:21 <br /> Sample ID: LCS MS09W0315A Units : pg/L Run ID: MSD_09_130315A Prep Date: 031151201310:21 <br /> Analyte Result PQL SpkVal SpkRefVal %REC LCL(ME) UCL(ME) RPDRefVal %RPD(Umit) Qual <br /> Benzene 9.95 0.5 10 100 70 130 <br /> Toluene 10.8 0.5 10 108 80 120 <br /> Ethylbenzene 10.7 0.5 10 107 80 120 <br /> m,p-Xylene 11 0.5 10 110 65 139 <br /> o-Xylene 11 .1 0.5 10 111 70 130 <br /> Surr: 1 ,2-Dichloroethane-d4 9.23 10 92 70 130 <br /> Sum: Toluene-d8 10.8 10 108 70 130 <br /> Sum: 4-Bromo0uombenzene 8.33 10 83 70 130 <br /> Sample Matrix Spike Type: MS Test Code: EPA Method SW8260B <br /> File ID: 13031519.13 Batch ID: MS09W0315A Analysis Date: 03/15/201316:03 <br /> Sample ID: 13031445-OSAMS Units : pg/L Run ID: MSD_09_130315A Prep Date: 03115/2013 16:03 <br /> Analyte Result PQL SpkVal SpkRefVal %REC LCL(ME) UCL(ME) RPDRefVal %RPD(Limit) Qual <br /> Benzene 53.5 1 .3 50 0 107 67 134 <br /> Toluene 54.9 1 .3 50 0 110 38 130 <br /> Ethylbenzene 53.9 1 .3 50 0 108 70 130 <br /> m ,p-Xylene 56.1 1 .3 50 0 112 65 139 <br /> o-Xylene 57 1 .3 50 0 114 69 130 <br /> Sum: 1 ,2-Dichloroethane-d4 48.3 50 97 70 130 <br /> Surr: Toluene-d8 54.6 50 109 70 130 <br /> Surr: 4-Bromoeuorobenzene 39.7 50 79 70 130 <br /> Sample Matrix Spike Duplicate Type: MSD Test Code: EPA Method SW8260B <br /> File ID: 13031520.D Batch ID: MS09W0315A Analysis Date: 03/15/2013 16:25 <br /> Sample ID: 13031445-05AMSD Units : pglL Run ID: MSD_09_130315A Prep Dale: 031151201316:25 <br /> Analyte Result PQL SpkVal SpkRefVal %REC LCL(ME) UCL(ME) RPDRefVal %RPD(Limit) Qual <br /> Benzene 54,5 1 .3 50 0 109 67 134 53.46 1 .9(21 ) <br /> Toluene 60,9 1 .3 50 0 122 38 130 54.92 10.2(20) <br /> Ethylbenzene 59.7 1 .3 50 0 119 70 130 53.9 10. 1 (20) <br /> m ,p-Xylene 61 .8 1 .3 50 0 124 65 139 56.07 9.7(20) <br /> o-Xylene 63. 1 1 .3 50 0 126 69 130 56.97 10.2(20) <br /> Surr: 1 ,2-Dichloroethane-d4 44.3 50 89 70 130 <br /> Surr: Toluene-d8 55.8 50 112 70 130 <br /> Surr: 4-Bromo0uorobenzene 40.6 50 81 70 130 <br />