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0 Report Number 40039 QC Report Matrix Spike/Matrix Spike Duplicate Date 9/16/2004 Project Name BARNES TRUCKING Project Number ZB178C Duplicate Spiked Duplicate Spiked Spiked Sample Relative Spike Spiked Spiked Sample Sample Relative Percent Percent Spiked Sample Spike Dup Sample Sample Analysis Date Percent Percent Percent Recov Diff Parameter Sample Value Level Level Value Value Units Method Analyzed Recov Recov Diff Limit Limit Benzene 39997-06 <0 50 388 38 7 396 398 ug/L EPA 8260B 9/13/04 102 103 0 879 70-130 25 Toluene 39997-06 <0 50 388 387 375 375 ug/L EPA 8260B 9/13/04 966 968 0 212 70-130 25 Tert-Butanol 39997-06 <5 0 194 193 190 192 ug/L EPA 8260B 9/13/04 98 0 994 141 70-130 25 Methyl-t-Butyl Ether 39997-06 <0 50 388 387 426 41 2 ug/L EPA 8260E 9/13104 110 106 2 96 70-130 25 Benzene 40039-01 38 400 400 714 682 ug/L EPA 8260B 9/14/04 836 754 103 70-130 25 Toluene 40039-01 70 400 400 101 101 ug/L EPA 8260B 9/14104 77 1 787 214 70-130 25 Tert-Butanol 40039-01 <5 0 200 200 200 204 ug/L EPA 82606 9/14104 998 102 208 70-130 25 Methyl-t-Butyl Ether40039-01 <0 50 400 400 363 358 ug/L EPA 8260B 9/14/04 907 895 128 70-130 25 Benzene 40039-06 47 400 400 870 81 0 ug/L EPA 82606 9/15/04 993 841 165 70-130 25 Toluene 40039-06 62 400 400 994 976 ug/L EPA 82606 9/15/04 94 6 901 4 92 70-130 25 Tert-Butanol 40039-06 <5 0 200 200 208 203 ug/L EPA 8260B 9/15/04 104 101 271 70-130 25 Methyl-t-Butyl Ether40039-06 <0 50 400 400 352 34 8 ug/L EPA 8260B 9/15/04 881 87 0 131 70-130 25 Benzene 40049-07 <0 50 400 400 396 373 ug/L EPA 8260B 9/15/04 991 93 3 597 70-130 25 Toluene 40049-07 <0 50 400 400 443 418 ug/L EPA 8260B 9/15/04 111 104 588 70-130 25 Tert-Butanol 40049-07 <50 200 200 203 200 ug/L EPA 82606 9/15/04 101 100 1 12 70-130 25 Methyl-t-Butyl Ether40049-07 <0 50 400 400 339 32 6 ug/L EPA 8260B 9/15/04 84 7 81 5 389 70-130 25 Approved By ,to iff KIFF ANALYTICAL, LLC 2795 2nd St, Suite 300 Davis, CA 95616 530-297-4800