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American Environmental Network <br /> WORK ORDER 9709391 QUALITY CONTROL REPORT PAGE QR-6 <br /> ANALYSIS Volatile GUMS <br /> MATRIX Soil/Bulk <br /> METHOD BLANK SAMPLES <br /> - - - -- - - ------- - -- ------ - ---------------- ---_ ------------- ------ - ----- ------ -- <br /> SAMPLE TYPE Blank Method/Media blank LAB ID BLNK 1009 INSTR RUN GCMS12\971009000000/1/ <br /> INSTRUMENT HP mass spec for Volatiles PREPARED BATCH ID MS12S100997 <br /> UNITS ug/kg ANALYZED 10/09/97 DILUTION 1 00 <br /> METHO <br /> REF REPORTING SPIKE RECOVERY REC LIMITS (X) RPD <br /> ANALYTE RESULT RESULT LIMIT VALUE (X) LOW HIGH RPD (X) LIMIT (X) <br /> 1 2-DCA d4 (surr) 98 1 100 98 1 80 137 <br /> Toluene d8 (surr) 104 100 104 84 116 <br /> p BFB (surr) 95 4 100 95 4 72 116 <br /> 1 1 Dichloroethene NO 5 <br /> Benzene NO 5 <br /> Trichloroethene NO 5 <br /> Toluene NO 5 <br /> Chlorobenzene NO 5 <br /> Acetone NO 100 <br /> Bromodichloromethane NO 5 <br /> Bromoform NO 5 <br /> Bromomethane NO 10 <br /> 2 Butanone NO 100 <br /> Carbon Disulfide ND 10 <br /> Carbon Tetrachloride NO 5 'J <br /> Chloroethane NO 10 <br /> 2-Chloroethyl Vinyl Ether NO 10 <br /> Chloroform NO 5 <br /> Chloromethane NO 10 <br /> Dibromochloromethane NO 5 <br /> 1 1 Dichloroethane ND 5 <br /> 1 2 Dichloroethane ND 5 <br /> • cis 1 2 Dichloroethene ND 5 <br /> trans 1 2 Dichloroethene NO 5 <br /> 1 2 Dichloropropane NO 5 <br /> cis 1 3 Di chl oropropene NO 5 <br /> trans 1 3 Dichloropropene NO 5 <br /> Ethylbenzene NO 5 <br /> 2 Hexanone NO 50 <br /> Methylene Chloride NO 10 <br /> 4 Methyl-2 pentanone NO 50 <br /> Styrene NO 5 <br /> 1,1,2 2 Tetrachloroethane NO 5 <br /> Tetrachloroethene NO 5 <br /> 1 1 1 Trichloroethane NO 5 <br /> 1 1 2 Trichloroethane NO 5 <br /> Vinyl Acetate NO 50 <br /> Vinyl Chloride NO 10 <br /> Xylenes Total NO 10 <br /> 1 2 Dibromoethane NO 5 <br /> Dichlorodifluoromethane NO 10 <br /> Trichlorofluoromethane NO 5 <br /> Trzchlorotrifluoroethane NO 5 <br /> Cyclohexane NO 5 <br /> Ethyl Acetate ND 5 <br /> Hexane ND 5 <br /> iso Octane ND 5 <br /> n Proppylbenzene ND 5 <br /> Tetrahydrofuran NO 50 <br /> -- --- <br /> - ---- <br /> -- --- -- --------- - ------------ -- -- - -- - -------- --- - --- -- ---- ---- ---------- -- <br /> SAMPLE TYPE Blank Method/Media blank LAB ID BLNK_1010 INSTR RUN GCMS13\971010010000/1/ <br /> INSTRUMENT HP mass spec for Volatiles PREPARED BATCH ID MS13SIO1197 <br /> UNITS ug/kg ANALYZED 10/10/97 DILUTION 1 00 <br /> METHOD <br /> REF REPORTING SPIKE RECOVERY REC LIMITS (X) RPD <br /> ANALYTE RESULT RESULT LIMIT VALUE (X) LOW HIGH RPD (X) LIMIT (X <br /> 1 2 DCA d4 (surr) 102 100 102 60 140 <br /> Toluene d8 (surr) 97 4 100 97 4 60 140 <br /> p BFB (surr) 92 1 100 92 1 60 140 <br /> 1 1 Dichloroethene NO <br /> Benzene ND <br /> Trichloroethene NO <br /> Toluene NO <br />