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American Environmental Network <br /> WORK ORDER 9799391 QUALITY CONTROL REPORT PAGE QR-9 <br /> • ANALYSIS- Volatile GUMS <br /> MATRIX- Soil/Bulk <br /> METHOD BLANK SAMPLES <br /> - ----- --- ------- --------------- --- <br /> .--- - - -- ---- --- - ------- ------- ----- ----- ------ ------ <br /> SAMPLE TYPE Blank-Method/Media blank LAB ID BLNK 1011 INSTR RUN GCMS131971010010000/4/ <br /> INSTRUMENT HP mass spec for Volatiles PREPARED — BATCH ID MS13S101197 <br /> UNITS ug/kg ANALYZED 10/11/97 DILUTION 1 00 <br /> METHOD <br /> REF REPORTING SPIKE RECOVERY REC LIMITS (X) RPD <br /> ANALYTE RESULT RESULT LIMIT VALUE (X) LOW HIGH RPD (X) LIMIT (X) <br /> 1 2 4 Trimethylbenzene ND <br /> 1,3 5 Trimethylbenzene ND <br /> Vinyl Chloride ND <br /> Xylenes, Total ND <br /> Trichlorotrifluoroethane ND <br /> Acetone ND <br /> Acrylonitrile ND <br /> 2 Butanone ND <br /> Carbon Disulfide ND <br /> trans 1 4 Dichloro 2 buten ND <br /> cis 1,3-Dichloropropene ND <br /> trans-1 3-Dichloropropene ND <br /> 2 Hexanone ND <br /> Methyl Iodide ND <br /> 4 Methyl 2-pentanone ND <br /> Vinyl Acetate ND <br /> 2 Chloroethyl Vinyl Ether ND <br /> -- -- - ------ ------- --------- - - - ---- -- - - ------ -------------_. <br /> SAMPLE TYPE Blank Method/Media blank LAB ID BLNK 1010 INSTR RUN GCMS131971010230000/1/ <br /> INSTRUMENT HP mass spec for Volatiles PREPARED BATCH ID MS13SIO1197 <br /> UNITS ug/kg ANALYZED 10/10/97 DILUTION 1 00 <br /> METHOD <br /> REF REPORTING SPIKE RECOVERY REC LIMITS (X) RPD <br /> ANALYTE RESULT RESULT LIMIT VALUE (X) LOW HIGH RPD (X) LIMIT (X) <br /> 1 2 DCA d4 (surr) 102 100 102 60 140 <br /> Toluene-d8 (surr) 97 4 100 97 4 60 140 <br /> p-BFB (surr) 92 1 100 92 1 60 140 <br /> 1 I-Dichloroethene ND <br /> Benzene ND <br /> Trichloroethene ND <br /> Toluene ND <br /> Chlorobenzene ND <br /> Bromobenzene ND <br /> Bromochloromethane ND <br /> Bromodichloromethane ND <br /> Bromoform ND <br /> Bromomethane ND <br /> n Butylbenzene ND <br /> sec Butylbenzene ND <br /> tert Butylbenzene ND <br /> Carbon Tetrachloride NO <br /> Chloroethane NO <br /> Chloroform NO <br /> Chloromethane ND <br /> 2 Chlorotoluene ND <br /> 4 Chlorotoluene NO <br /> Dibromochloromethane NO <br /> 1 2 Dibromo-3 chloropropan ND <br /> 1 2 Dibromoethane ND <br /> Dibromomethane ND <br /> 1 2 Dichlorobenzene ND <br /> 1 3 Dichlorobenzene ND <br /> 1 4 Dichlorobenzene ND <br /> Dichlorodifluoromethane ND <br /> 1 1 Dzchloroethane ND <br /> 1 2 Dichloroethane NO <br /> . cis 1 2 Dichloroethene NO <br /> trans 1 2 Dichloroethene NO <br /> 1 2 Dzchloropropane ND <br /> 1 3 Dzchloropropane ND <br /> 2 2 Dzchloropropane ND <br /> 1 1 Dichloropropene ND <br /> Ethylbenzene NO <br />